2-(alpha-Acetoxy-2-methoxybenzyl)propenoic acid methyl ester

Base Information

Chemical Name:2-(alpha-Acetoxy-2-methoxybenzyl)propenoic acid methyl ester
CAS No.:124957-37-5
Molecular Formula:C14H16O5
Molecular Weight:264.278
Hs Code.:
DSSTox Substance ID:DTXSID801187861
Nikkaji Number:J1.506.389K

Synonyms:DTXSID801187861;2-(alpha-Acetoxy-2-methoxybenzyl)propenoic acid methyl ester;Methyl beta-(acetyloxy)-2-methoxy-alpha-methylenebenzenepropanoate;124957-37-5

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Chemical Property of 2-(alpha-Acetoxy-2-methoxybenzyl)propenoic acid methyl ester

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:7
Exact Mass:264.09977361
Heavy Atom Count:19
Complexity:350

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)OC(C1=CC=CC=C1OC)C(=C)C(=O)OC

Technology Process of 2-(alpha-Acetoxy-2-methoxybenzyl)propenoic acid methyl ester

There total 3 articles about 2-(alpha-Acetoxy-2-methoxybenzyl)propenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 115240-90-9
methyl 2-(hydroxy(2-methoxyphenyl)methyl)acrylate

: 75-36-5
acetyl chloride

: 124957-37-5
2-[Acetoxy-(2-methoxy-phenyl)-methyl]-acrylic acid methyl ester

Guidance literature:: With triethylamine; at 20 ℃; for 2h;

Reference yield: 5.0%

: 124957-43-3
methyl (2E)-2-(acetoxymethyl)-3-(2-methoxyphenyl)prop-2-enoate

: 124957-37-5
2-[Acetoxy-(2-methoxy-phenyl)-methyl]-acrylic acid methyl ester

: 124957-57-9
(E)-3-(2-Methoxy-phenyl)-2-phenylaminomethyl-acrylic acid methyl ester

Guidance literature:: With aniline; In tetrahydrofuran; for 0.5h;

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 124957-37-5
2-[Acetoxy-(2-methoxy-phenyl)-methyl]-acrylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / diaza-1,4 bicyclo<2.2.2> octane / 480 h / 20 °C

2: 85 percent / triethylamine / 2 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; triethylamine;