1,2-Difluoro-3-propylbenzene

Base Information

Chemical Name:1,2-Difluoro-3-propylbenzene
CAS No.:126163-01-7
Molecular Formula:C9H10F2
Molecular Weight:156.175
Hs Code.:
DSSTox Substance ID:DTXSID40560991
Wikidata:Q82444651

Synonyms:1,2-difluoro-3-propylbenzene;126163-01-7;3-propyl-1,2-difluorobenzene;SCHEMBL4476574;DTXSID40560991;SUJZXHZDAHNHQZ-UHFFFAOYSA-N

Suppliers and Price of 1,2-Difluoro-3-propylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,2-Difluoro-3-propylbenzene

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:156.07505664
Heavy Atom Count:11
Complexity:114

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCCC1=C(C(=CC=C1)F)F

Technology Process of 1,2-Difluoro-3-propylbenzene

There total 5 articles about 1,2-Difluoro-3-propylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 367-11-3
ortho-difluorobenzene

: 107-08-4
1-iodo-propane

: 126163-01-7
2,3-difluoro-1-n-propylbenzene

Guidance literature:: ortho-difluorobenzene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran;

1-iodo-propane; With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; In tetrahydrofuran; Further stages.;
DOI:10.1021/jm070111+

Reference yield:

: 127860-79-1
1,2-Difluoro-3-((E)-propenyl)-benzene

: 126163-01-7
2,3-difluoro-1-n-propylbenzene

Guidance literature:: With hydrogen; platinum(IV) oxide; In pentane; for 12h; under 760 Torr;
DOI:10.1039/b212107g

Reference yield:

: 367-11-3
ortho-difluorobenzene

: 126163-01-7
2,3-difluoro-1-n-propylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / 1.5 h / -78 °C

1.2: 96 percent / tetrahydrofuran / -78 - 20 °C

2.1: P₂O₅ / pentane

3.1: 46.3 g / H₂ / PtO₂ / pentane / 12 h / 760 Torr

With hydrogen; phosphorus pentoxide; lithium diisopropyl amide; platinum(IV) oxide; In tetrahydrofuran; pentane;
DOI:10.1039/b212107g