4-(6-Methyl-1,3,6,2-dioxazaborocan-2-yl)benzaldehyde

Base Information

Chemical Name:4-(6-Methyl-1,3,6,2-dioxazaborocan-2-yl)benzaldehyde
CAS No.:128376-66-9
Molecular Formula:C12H16BNO3
Molecular Weight:233.075
Hs Code.:
DSSTox Substance ID:DTXSID90560643
Nikkaji Number:J566.816F
Wikidata:Q82444113
Mol file:128376-66-9.mol

Synonyms:128376-66-9;4-(6-Methyl-1,3,6,2-dioxazaborocan-2-yl)benzaldehyde;Benzaldehyde, 4-(tetrahydro-6-methyl-4H-1,3,6,2-dioxazaborocin-2-yl)-;N-methyliminodiethyl 4-formylbenzeneboronate;DTXSID90560643;AS-76853;D92864

Suppliers and Price of 4-(6-Methyl-1,3,6,2-dioxazaborocan-2-yl)benzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 4-(6-Methyl-1,3,6,2-dioxazaborocan-2-yl)benzaldehyde

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:233.1223235
Heavy Atom Count:17
Complexity:234

Purity/Quality:: 99%,98%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B1(OCCN(CCO1)C)C2=CC=C(C=C2)C=O

Technology Process of 4-(6-Methyl-1,3,6,2-dioxazaborocan-2-yl)benzaldehyde

There total 1 articles about 4-(6-Methyl-1,3,6,2-dioxazaborocan-2-yl)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 105-59-9
N-Methyldiethanolamine

: 87199-17-5
4-formylphenylboronic acid,

: 128376-66-9
N-methyliminodiethyl 4-formylbenzeneboronate

Guidance literature:: In toluene; at 20 ℃; for 5h; Molecular sieve;
DOI:10.1016/j.bmc.2012.11.055

Reference yield: 83.0%

: 128376-66-9
N-methyliminodiethyl 4-formylbenzeneboronate

: 14235-81-5
4-Ethynylaniline

: N-methyliminodiethyl 4-((E)-4-ethynylphenyliminomethyl)benzeneboronate

Guidance literature:: With pyridinium p-toluenesulfonate; for 16h; Heating;
DOI:10.1007/s00706-005-0398-4

Reference yield:

: 128376-66-9
N-methyliminodiethyl 4-formylbenzeneboronate

: N-methyliminodiethyl 4-(cyano-(4-ethynylphenylamino)methyl)benzeneboronate

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / pyridinium 4-toluenesulfonate / 16 h / Heating

2: 87 percent / scandium triflate / CH₂Cl₂ / 16 h / 20 °C

With pyridinium p-toluenesulfonate; scandium tris(trifluoromethanesulfonate); In dichloromethane;
DOI:10.1007/s00706-005-0398-4