5-Hexenoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-2-(trifluoromethyl)-, methyl ester

Base Information

Chemical Name:5-Hexenoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-2-(trifluoromethyl)-, methyl ester
CAS No.:129398-27-2
Molecular Formula:C16H18F3NO4
Molecular Weight:345.31400
Hs Code.:

Synonyms:2-Benzyloxycarbonylamino-2-trifluoromethyl-hex-5-enoic acid methyl ester;

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Chemical Property of 5-Hexenoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-2-(trifluoromethyl)-, methyl ester

Chemical Property:

PSA：64.63000
LogP:3.74400

Purity/Quality:

Safty Information:

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Technology Process of 5-Hexenoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-2-(trifluoromethyl)-, methyl ester

There total 2 articles about 5-Hexenoic acid, 2-[[(phenylmethoxy)carbonyl]amino]-2-(trifluoromethyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 7103-09-5
4-but-1-enylmagnesium bromide

: 128970-26-3
methyl 2-benzyloxycarbonylimino-3,3,3-trifluoropropionate

: 129398-27-2
methyl 2-(benzyloxycarbonylamino)-2-(trifluoromethyl)hex-5-enoate

Guidance literature:: In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1002/1099-0690(200110)2001:20<3891::AID-EJOC3891>3.0.CO;2-R

Reference yield:

: 5162-44-7
1-bromo-4-butene

: 276862-98-7
2-[(E)-Benzyloxycarbonylimino]-3,3,3-trifluoro-propionic acid methyl ester

: 129398-27-2
methyl 2-(benzyloxycarbonylamino)-2-(trifluoromethyl)hex-5-enoate

Guidance literature:: With magnesium; Yield given. Multistep reaction; 1.) Et₂O, -70 deg C, 2.) Et₂O, -70 deg C to r.t.;
DOI:10.1016/S0022-1139(96)03461-6