1-[3-(Triethoxysilyl)propyl]-1H-imidazole

Base Information

• Chemical Name: 1-[3-(Triethoxysilyl)propyl]-1H-imidazole
• CAS No.: 63365-92-4
• Molecular Formula: C12H24N2O3Si
• Molecular Weight: 272.42
• European Community (EC) Number: 264-111-8
• DSSTox Substance ID: DTXSID70979512
• Nikkaji Number: J349.163C
• Wikidata: Q82965173
• Mol file: 63365-92-4.mol

Synonyms:63365-92-4;1-[3-(TRIETHOXYSILYL)PROPYL]-1H-IMIDAZOLE;triethoxy(3-imidazol-1-ylpropyl)silane;EINECS 264-111-8;1-(3-(Triethoxysilyl)propyl)-1H-imidazole;C12H24N2O3Si;SCHEMBL485757;DTXSID70979512;C12-H24-N2-O3-Si;n-(3-triethoxysilylpropyl)imidazole;MFCD23103244;1-[3-(Triethyloxysilyl)propyl]imidazole;1H-Imidazole, 1-[3-(triethoxysilyl)propyl)]

Chemical Property of 1-[3-(Triethoxysilyl)propyl]-1H-imidazole

Chemical Property:

• Vapor Pressure: 0.000175mmHg at 25°C
• Boiling Point: 339.9°Cat760mmHg
• PKA: 7.04±0.10(Predicted)
• Flash Point: 159.4°C
• Density: 1.01g/cm³
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 10
• Exact Mass: 272.15561917
• Heavy Atom Count: 18
• Complexity: 203

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCO[Si](CCCN1C=CN=C1)(OCC)OCC

Technology Process of 1-[3-(Triethoxysilyl)propyl]-1H-imidazole

There total 3 articles about 1-[3-(Triethoxysilyl)propyl]-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1H-imidazole (288-32-4) + (3-chloropropyl)triethoxysilane (5089-70-3) → 3-(2-imidazolin-1-yl)propyltriethoxysilane (63365-92-4)

Guidance literature:

1H-imidazole; With sodium ethanolate; In tetrahydrofuran; at 20 ℃; for 1.33333h; Large scale;

(3-chloropropyl)triethoxysilane; In tetrahydrofuran; at 100 - 120 ℃; for 3h; Large scale;

Reference yield: 70.0%

1H-imidazole (288-32-4) + (3-iodopropyl)triethoxysilane (57483-09-7) → 3-(2-imidazolin-1-yl)propyltriethoxysilane (63365-92-4)

Guidance literature:

1H-imidazole; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

(3-iodopropyl)triethoxysilane; In tetrahydrofuran; at 0 - 75 ℃;

DOI:10.1039/b812607k

Reference yield:

(3-chloropropyl)triethoxysilane (5089-70-3) + imidazolyl sodium (5587-42-8) → 3-(2-imidazolin-1-yl)propyltriethoxysilane (63365-92-4)

Guidance literature:

In ethanol; for 12h; Reflux; Inert atmosphere;

DOI:10.1016/j.molcata.2011.08.005

upstream raw materials:

1H-imidazole

(3-iodopropyl)triethoxysilane

(3-chloropropyl)triethoxysilane

imidazolyl sodium

Downstream raw materials:

C₃₄H₄₆N₃O₉Si⁽¹⁺⁾*Cl^(1-)