Benzyl 3-(3,4-bis(benzyloxy)phenyl)acrylate

Base Information

Chemical Name:Benzyl 3-(3,4-bis(benzyloxy)phenyl)acrylate
CAS No.:91174-00-4
Molecular Formula:C30H26O4
Molecular Weight:450.525
Hs Code.:
NSC Number:175295
ChEMBL ID:CHEMBL1986088

Synonyms:Benzyl 3-(3,4-bis(benzyloxy)phenyl)acrylate;91174-00-4;NSC175295;NSC 175295;CHEMBL1986088;NSC-175295;benzyl (E)-3-(3,4-dibenzyloxyphenyl)prop-2-enoate

Suppliers and Price of Benzyl 3-(3,4-bis(benzyloxy)phenyl)acrylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Benzyl 3-(3,4-bis(benzyloxy)phenyl)acrylate

Chemical Property:

Vapor Pressure:3.35E-15mmHg at 25°C
Boiling Point:618°Cat760mmHg
Flash Point:263.5°C
Density:1.183g/cm³
XLogP3:6.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:11
Exact Mass:450.18310931
Heavy Atom Count:34
Complexity:599

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC2=C(C=C(C=C2)C=CC(=O)OCC3=CC=CC=C3)OCC4=CC=CC=C4
Isomeric SMILES:C1=CC=C(C=C1)COC2=C(C=C(C=C2)/C=C/C(=O)OCC3=CC=CC=C3)OCC4=CC=CC=C4

Technology Process of Benzyl 3-(3,4-bis(benzyloxy)phenyl)acrylate

There total 1 articles about Benzyl 3-(3,4-bis(benzyloxy)phenyl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 331-39-5,501-16-6
caffeic acid

: 100-39-0
benzyl bromide

: 91174-00-4
benzyl 3,4-dibenzyloxycinnamate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 15h; Inert atmosphere;
DOI:10.1007/s11746-011-1889-6

Reference yield: 94.0%

: 91174-00-4
benzyl 3,4-dibenzyloxycinnamate

: 54429-62-8
(3,4-di(benzyloxy)phenyl)prop-2-enoic acid

Guidance literature:: With methanol; sodium hydroxide; at 70 ℃; for 4h;

Reference yield:

: 91174-00-4
benzyl 3,4-dibenzyloxycinnamate

: C₂₃H₂₈O₆

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / ethanol; water / 2 h / Reflux

2: dmap; dicyclohexyl-carbodiimide / ethanol; dichloromethane / 15 h / 20 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / tetrahydrofuran / 24 h / 20 °C

With dmap; palladium 10% on activated carbon; hydrogen; dicyclohexyl-carbodiimide; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1007/s11746-011-1889-6