Carbamic acid, [1-(diphenoxyphosphinyl)butyl]-, phenylmethyl ester

Base Information

Chemical Name:Carbamic acid, [1-(diphenoxyphosphinyl)butyl]-, phenylmethyl ester
CAS No.:130727-16-1
Molecular Formula:C24H26NO5P
Molecular Weight:439.448
Hs Code.:
DSSTox Substance ID:DTXSID80407391
Nikkaji Number:J2.321.029K

Synonyms:Carbamic acid, [1-(diphenoxyphosphinyl)butyl]-, phenylmethyl ester;130727-16-1;DTXSID80407391;PD136134

Suppliers and Price of Carbamic acid, [1-(diphenoxyphosphinyl)butyl]-, phenylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Carbamic acid, [1-(diphenoxyphosphinyl)butyl]-, phenylmethyl ester

Chemical Property:

XLogP3:5.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:11
Exact Mass:439.15485993
Heavy Atom Count:31
Complexity:544

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(NC(=O)OCC1=CC=CC=C1)P(=O)(OC2=CC=CC=C2)OC3=CC=CC=C3

Technology Process of Carbamic acid, [1-(diphenoxyphosphinyl)butyl]-, phenylmethyl ester

There total 3 articles about Carbamic acid, [1-(diphenoxyphosphinyl)butyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 101-02-0
triphenyl phosphite

: 621-84-1
O-benzyl carbamate

: 123-72-8
butyraldehyde

: 130727-16-1
benzyl N-[1-(diphenoxyphosphoryl)butyl]carbamate

Guidance literature:: With acetic acid; at 80 - 90 ℃; for 2h;
DOI:10.1016/j.bmc.2019.07.049

Reference yield:

: 621-84-1
O-benzyl carbamate

: 115-86-6
phosphoric acid triphenyl ester

: 123-72-8
butyraldehyde

: 130727-16-1
benzyl N-[1-(diphenoxyphosphoryl)butyl]carbamate

Guidance literature:: With tetrafluoroboric acid; In methanol; diethyl ether; at 20 ℃; for 4.5h; Cooling with ice;
DOI:10.1021/jacs.7b04394

Reference yield:

: 108-95-2,27073-41-2
phenol

: 130727-16-1
benzyl N-[1-(diphenoxyphosphoryl)butyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride / acetonitrile / 6 h / Reflux

2: acetic acid / 2 h / 80 - 90 °C

With acetic acid; phosphorus trichloride; In acetonitrile;
DOI:10.1021/jm300599x