Benzenetridecanoic acid, 4-methoxy-

Base Information

Chemical Name:Benzenetridecanoic acid, 4-methoxy-
CAS No.:13099-37-1
Molecular Formula:C₂₀H₃₂O₃
Molecular Weight:320.472
Hs Code.:

Synonyms:

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Chemical Property of Benzenetridecanoic acid, 4-methoxy-

Chemical Property:

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Technology Process of Benzenetridecanoic acid, 4-methoxy-

There total 11 articles about Benzenetridecanoic acid, 4-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50889-29-7
(5-carboxypentyl)triphenylphosphonium bromide

: 13099-37-1
13-(4'-methoxyphenyl)tridecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuOK / 1.) THF, 0 deg C, 20 min, 2.) THF, 50 min, RT

2: H₂ / Pd/C / ethanol

With potassium tert-butylate; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1248/cpb.45.685

Reference yield:

: (6E,12E)-13-(4-Methoxy-phenyl)-trideca-6,12-dienoic acid

: 13099-37-1
13-(4'-methoxyphenyl)tridecanoic acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; Yield given;
DOI:10.1248/cpb.45.685

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 13099-37-1
13-(4'-methoxyphenyl)tridecanoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) t-BuOK / 1.) THF, 0 deg C, 20 min, 2.) THF, RT

2: LiAlH₄ / tetrahydrofuran / 1.5 h / 0 °C

3: 1.) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, 20 min, 2.) CH₂Cl₂, 30 min, RT

4: 1.) t-BuOK / 1.) THF, 0 deg C, 20 min, 2.) THF, 50 min, RT

5: H₂ / Pd/C / ethanol

With lithium aluminium tetrahydride; oxalyl dichloride; potassium tert-butylate; hydrogen; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol;
DOI:10.1248/cpb.45.685