6-Heptenoic acid, 7-phenyl-, (6E)-

Base Information

• Chemical Name: 6-Heptenoic acid, 7-phenyl-, (6E)-
• CAS No.: 13159-14-3
• Molecular Formula: C13H16O2
• Molecular Weight: 204.269

Synonyms:

Chemical Property of 6-Heptenoic acid, 7-phenyl-, (6E)-

Chemical Property:

Purity/Quality:

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Technology Process of 6-Heptenoic acid, 7-phenyl-, (6E)-

There total 7 articles about 6-Heptenoic acid, 7-phenyl-, (6E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

7-oxooctanoic acid (14112-98-2) + benzaldehyde (100-52-7) → (E)-7-phenyl-6-heptenoic acid (13159-14-3) + acetic acid (64-19-7,77671-22-8)

Guidance literature:

With ytterbium(III) triflate; at 60 ℃; for 8h;

DOI:10.1002/ejoc.200300076

Reference yield: 14.0%

N-2,2,6,6-tetramethylpiperidinyl 2-(N-2,2,6,6-tetramethyl-piperidinyloxy)-7-phenyl-5-heptenoate → 2,2,6,6-tetramethyl-piperidine (768-66-1) + 7c-Phenyl-hept-6-ensaeure (13159-20-1) + (E)-7-phenyl-6-heptenoic acid (13159-14-3)

Guidance literature:

In tert-butyl alcohol; at 132 - 135 ℃; for 18h; Title compound not separated from byproducts;

DOI:10.1139/v03-076

Reference yield: 7.0%

N-2,2,6,6-tetramethylpiperidinyl 2-(N-2,2,6,6-tetramethyl-piperidinyloxy)-7-phenyl-5-heptenoate → 7c-Phenyl-hept-6-ensaeure (13159-20-1) + (E)-7-phenyl-6-heptenoic acid (13159-14-3) + 2-(phenyl-N-2,2,6,6-tetramethylpiperidinyloxymethyl)cyclopentanecarboxylic acid

Guidance literature:

In tert-butyl alcohol; at 130 ℃; for 10h; Title compound not separated from byproducts;

DOI:10.1139/v03-076

upstream raw materials:

diethyl (E)-2-(5-phenylpent-4-enyl)malonate

7-oxooctanoic acid

benzaldehyde

(4E)-5-phenyl-4-pentenoic acid

Downstream raw materials:

7-(2-hydroxy-3,4,6-trimethylphenyl)-7-phenylheptanoic acid

7-(4-fluorophenyl)-7-(3-formyl-6-hydroxy-2,4,5-trimethylphenyl)heptanoic acid

(S)-5-(4-Benzyloxy-phenyl)-4-(7-phenyl-heptanoylamino)-pentanoic acid methyl ester

C₂₀H₁₉N₃O

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