2-Butyl-2,3-dihydro-1H-1,3,2-benzodiazaborole

Base Information

• Chemical Name: 2-Butyl-2,3-dihydro-1H-1,3,2-benzodiazaborole
• CAS No.: 31748-14-8
• Molecular Formula: C10H15 B N2
• Molecular Weight: 174.053
• Hs Code.: 2934999090
• Mol file: 31748-14-8.mol

Synonyms:2H-1,3,2-Benzodiazaborole,2-butyl-1,3-dihydro- (6CI); NSC 405003; o-Phenylenediamine cyclicbutaneboronate

Chemical Property of 2-Butyl-2,3-dihydro-1H-1,3,2-benzodiazaborole

Chemical Property:

• Vapor Pressure: 0.0075mmHg at 25°C
• Boiling Point: 268.9°Cat760mmHg
• Flash Point: 116.4°C
• PSA: 24.06000
• Density: 0.99g/cm³
• LogP: 3.08830

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Butyl-2,3-dihydro-1H-1,3,2-benzodiazaborole

There total 1 articles about 2-Butyl-2,3-dihydro-1H-1,3,2-benzodiazaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

butylborane; compound with trimethylamine (1:1) + 1,2-diamino-benzene (95-54-5) → 2-butyl-2,3-dihydro-1H-benzo[1,3,2]diazaborole (31748-14-8) + trimethylamine (75-50-3)

Guidance literature:

In benzene; byproducts: H2; reflux, then cooling and adding pentane to the mixture; recrystn. from benzene-pentane;

DOI:10.1021/ja01465a022 DOI:10.1021/ja01530a077

upstream raw materials:

1,2-diamino-benzene

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