Technology Process of Benzamide,
4-formyl-N-methyl-N-[(5-methyl-2-phenyl-4-oxazolyl)methyl]-
There total 7 articles about Benzamide,
4-formyl-N-methyl-N-[(5-methyl-2-phenyl-4-oxazolyl)methyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 40 percent / H2 / 10percent Pd/C / ethanol; methanol / 3 h / 2585.7 Torr
2: 84 percent / LiAlH4 / diethyl ether / 1 h / Ambient temperature
3: 70 percent / pyridinium dichromate / CH2Cl2 / 7 h
4: MgSO4 / diethyl ether / 1.) 0 deg C, 15 min, 2.) RT, 3 h
5: sodium borohydride / diethyl ether / 1.) 0 deg C, 15 min, 2.) RT, 18 h
6: tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) RT, overnight
With
sodium tetrahydroborate; lithium aluminium tetrahydride; dipyridinium dichromate; hydrogen; magnesium sulfate;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm00088a022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 70 percent / pyridinium dichromate / CH2Cl2 / 7 h
2: MgSO4 / diethyl ether / 1.) 0 deg C, 15 min, 2.) RT, 3 h
3: sodium borohydride / diethyl ether / 1.) 0 deg C, 15 min, 2.) RT, 18 h
4: tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) RT, overnight
With
sodium tetrahydroborate; dipyridinium dichromate; magnesium sulfate;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jm00088a022
- Guidance literature:
-
Multi-step reaction with 3 steps
1: MgSO4 / diethyl ether / 1.) 0 deg C, 15 min, 2.) RT, 3 h
2: sodium borohydride / diethyl ether / 1.) 0 deg C, 15 min, 2.) RT, 18 h
3: tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) RT, overnight
With
sodium tetrahydroborate; magnesium sulfate;
In
tetrahydrofuran; diethyl ether;
DOI:10.1021/jm00088a022
