Borane, chlorobis(4-methylphenyl)-

Base Information

Chemical Name:Borane, chlorobis(4-methylphenyl)-
CAS No.:13272-74-7
Molecular Formula:C14H14BCl
Molecular Weight:228.529
Hs Code.:
DSSTox Substance ID:DTXSID40477676

Synonyms:Borane, chlorobis(4-methylphenyl)-;13272-74-7;SCHEMBL8629317;DTXSID40477676

Suppliers and Price of Borane, chlorobis(4-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Borane, chlorobis(4-methylphenyl)-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:228.0877083
Heavy Atom Count:16
Complexity:181

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:B(C1=CC=C(C=C1)C)(C2=CC=C(C=C2)C)Cl

Technology Process of Borane, chlorobis(4-methylphenyl)-

There total 4 articles about Borane, chlorobis(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1213-36-1
bis(4-methylphenyl)dimethylstannane

: 10294-34-5
boron trichloride

: 13272-74-7
bis(p-tolyl)boron chloride

Guidance literature:: In n-heptane; byproducts: dimethyltin dichloride; glovebox; addn. of 1 equiv. of BCl3 as 1 M soln. in heptane to a flask contg. dimethyldiaryltin and heptane at room temp., sealing, stirring at room temp. for 30 min, heating at 100°C in oil bath for 24-48 h; cooling, decantation, removal of volatiles, recrystn. from petroleum ether at -35°C;
DOI:10.1021/ic034150x