Technology Process of Phenol, 3-methoxy-4-(3-methyl-2-butenyl)-5-(2-phenylethyl)-
There total 11 articles about Phenol, 3-methoxy-4-(3-methyl-2-butenyl)-5-(2-phenylethyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 96.4 percent / H2 / 10percent Pd-C / ethyl acetate / 2 h / Ambient temperature
2: 919.1 mg / KI, K2CO3 / acetone / 43 h / 80 °C
3: 84.5 percent / H2, quinoline / Pd-BaSO4 / ethyl acetate
4: 13.5 percent / silica gel / hexane; benzene / 12 h / Ambient temperature; or in xylene at 130 deg C, 16 h
5: 88.3 percent / K2CO3 / acetone
6: 28.1 percent / EtSNa / dimethylformamide / 3 h / 170 - 180 °C
With
quinoline; hydrogen; silica gel; potassium carbonate; potassium iodide; sodium thioethylate;
palladium on activated charcoal; palladium on barium sulfate;
In
hexane; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/0031-9422(91)84129-G
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 919.1 mg / KI, K2CO3 / acetone / 43 h / 80 °C
2: 84.5 percent / H2, quinoline / Pd-BaSO4 / ethyl acetate
3: 13.5 percent / silica gel / hexane; benzene / 12 h / Ambient temperature; or in xylene at 130 deg C, 16 h
4: 88.3 percent / K2CO3 / acetone
5: 28.1 percent / EtSNa / dimethylformamide / 3 h / 170 - 180 °C
With
quinoline; hydrogen; silica gel; potassium carbonate; potassium iodide; sodium thioethylate;
palladium on barium sulfate;
In
hexane; ethyl acetate; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/0031-9422(91)84129-G
