Benzeneselenol, 2-amino-, zinc salt (2:1)

Base Information

• Chemical Name: Benzeneselenol, 2-amino-, zinc salt (2:1)
• CAS No.: 134174-55-3
• Molecular Formula: C6H7NSe.1/2Zn
• Molecular Weight: 407.551
• Mol file: 134174-55-3.mol

Synonyms:

Chemical Property of Benzeneselenol, 2-amino-, zinc salt (2:1)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneselenol, 2-amino-, zinc salt (2:1)

There total 5 articles about Benzeneselenol, 2-amino-, zinc salt (2:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

bis(o-nitrophenyl) diselenide (35350-43-7) + zinc (7440-66-6) → zinc 2-aminobenzeneselenolate (134174-55-3)

Guidance literature:

In acetic acid; elem. anal.;

Reference yield:

bis(o-nitrophenyl) diselenide (35350-43-7) → zinc 2-aminobenzeneselenolate (134174-55-3)

Guidance literature:

With acetic acid; zinc;

Reference yield:

2-nitro-aniline (88-74-4) → zinc 2-aminobenzeneselenolate (134174-55-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 0.25 h / -15 - -10 °C

1.2: 1 h / -10 - 0 °C

1.3: 0.5 h / Cooling with ice

2.1: sodium / ethanol / 1 h / Cooling with ice

3.1: acetic acid / 2 h / 100 °C

With boron trifluoride diethyl etherate; sodium; acetic acid; In ethanol; dichloromethane;

upstream raw materials:

bis(o-nitrophenyl) diselenide

zinc

2-nitro-aniline

ortho-nitrophenyl selenocyanate

Downstream raw materials:

2-methylbenzoselenazole

2-phenylbenzo[d][1,3]selenazole

2-(methylselanyl)aniline

2-benzoselenazol-2-yl-benzoic acid