Phosphoric acid, 4-(1,1-dimethylethyl)phenyl diethyl ester

Base Information

Chemical Name:Phosphoric acid, 4-(1,1-dimethylethyl)phenyl diethyl ester
CAS No.:13538-40-4
Molecular Formula:C14H23O4P
Molecular Weight:286.308
Hs Code.:
Mol file:13538-40-4.mol

Synonyms:

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Chemical Property of Phosphoric acid, 4-(1,1-dimethylethyl)phenyl diethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Phosphoric acid, 4-(1,1-dimethylethyl)phenyl diethyl ester

There total 3 articles about Phosphoric acid, 4-(1,1-dimethylethyl)phenyl diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 98-54-4
para-tert-butylphenol

: 762-04-9
phosphonic acid diethyl ester

: 13538-40-4
Phosphorsaeure-(4-tert-butylphenylester)-diethylester

Guidance literature:: With sodium iodide; In acetonitrile; at 20 ℃; for 2h; Electrochemical reaction; Green chemistry;
DOI:10.1039/d1ob00779c

Reference yield: 67.0%

: 64-17-5
ethanol

: 18351-36-5
4-tert-Butylphenoxy dichlorophosphate

: 13538-40-4
Phosphorsaeure-(4-tert-butylphenylester)-diethylester

Guidance literature:: With triethylamine; In diethyl ether; Petroleum ether; 1) 0 deg C; 2) 18h, 20 deg C; 3) 90 min reflux;

Reference yield:

: 98-54-4
para-tert-butylphenol

: 13538-40-4
Phosphorsaeure-(4-tert-butylphenylester)-diethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / 1) POCl₃, triethylamine / diethyl ether; petroleum ether / 1) 0 deg C, 3h; 2) 12h, 20 deg C; 3) 3h, reflux

2: 67 percent / triethylamine / diethyl ether; petroleum ether / 1) 0 deg C; 2) 18h, 20 deg C; 3) 90 min reflux

With triethylamine; trichlorophosphate; In diethyl ether; Petroleum ether;