Dibenzothiophene, 1-(phenylthio)-

Base Information

Chemical Name:Dibenzothiophene, 1-(phenylthio)-
CAS No.:135489-54-2
Molecular Formula:C18H12S2
Molecular Weight:292.425
Hs Code.:
Mol file:135489-54-2.mol

Synonyms:

Suppliers and Price of Dibenzothiophene, 1-(phenylthio)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dibenzothiophene, 1-(phenylthio)-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of Dibenzothiophene, 1-(phenylthio)-

There total 7 articles about Dibenzothiophene, 1-(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 908242-65-9
2-fluorophenyl-2-iodophenyl thio ether

: 882-33-7
diphenyldisulfane

: 135489-54-2
1-phenylthiodibenzothiophene

Guidance literature:: 2-fluorophenyl-2-iodophenyl thio ether; With tert.-butyl lithium; In tetrahydrofuran; pentane; for 0.833333h; cooling;

diphenyldisulfane; In tetrahydrofuran; pentane; for 0.5h; cooling;
DOI:10.1021/jo060911c

Reference yield: 45.0%

: 135489-36-0
4-phenylthiothianthrene-5-oxide

: 2974-10-9
1,3-bis(phenylthio)benzene

: 135489-54-2
1-phenylthiodibenzothiophene

Guidance literature:: With n-butyllithium;
DOI:10.3987/COM-91-5683

Reference yield:

: 2557-78-0
2-fluorothiophenol

: 135489-54-2
1-phenylthiodibenzothiophene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 78 percent / copper(I) oxide; pyridine / 12 h / Heating

2.1: 90 percent / HCl; iron / ethanol / 6 h / Heating

3.1: H₂SO₄; NaNO₂ / H₂O / 0.5 h / cooling

3.2: 72 percent / KI; copper / H₂O / 0.5 h / Heating

4.1: t-BuLi / tetrahydrofuran; pentane / 0.83 h / cooling

4.2: 78 percent / tetrahydrofuran; pentane / 0.5 h / cooling

With pyridine; copper(I) oxide; hydrogenchloride; sulfuric acid; tert.-butyl lithium; iron; sodium nitrite; In tetrahydrofuran; ethanol; water; pentane;
DOI:10.1021/jo060911c