3-Iodo-2,6-diMethylbenzenaMine.HCl

Base Information

• Chemical Name: 3-Iodo-2,6-diMethylbenzenaMine.HCl
• CAS No.: 135630-62-5
• Molecular Formula: C8H10IN.ClH
• Molecular Weight: 283.53700
• Mol file: 135630-62-5.mol

Synonyms:Benzenamine,3-iodo-2,6-dimethyl-,hydrochloride;3-Iodo-2,6-dimethylaniline hydrochloride;

Chemical Property of 3-Iodo-2,6-diMethylbenzenaMine.HCl

Chemical Property:

• Melting Point: 185-186 °C(Solv: methanol (67-56-1))
• PSA: 26.02000
• LogP: 3.87340
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

98%min ^*data from raw suppliers

3-Iodo-2,6-dimethylaniline hydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Iodo-2,6-diMethylbenzenaMine.HCl

There total 2 articles about 3-Iodo-2,6-diMethylbenzenaMine.HCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-iodo-2,4-dimethyl-3-nitro-benzene (56404-21-8) → 3-iodo-2,6-dimethylaniline hydrochloride (135630-62-5)

Guidance literature:

With hydrogenchloride; iron; Multistep reaction;

DOI:10.1248/cpb.39.1085

Reference yield:

2,6-dimethylnitrobenzene (81-20-9) → 3-iodo-2,6-dimethylaniline hydrochloride (135630-62-5)

Guidance literature:

Multi-step reaction with 2 steps

1: I₂, HIO₄

2: 1) Fe, 2) HCl

With hydrogenchloride; iodine; iron; periodic acid;

DOI:10.1248/cpb.39.1085

Reference yield: 74.0%

methanol (67-56-1) + 3-iodo-2,6-dimethylaniline hydrochloride (135630-62-5) → 3-iodo-2,6-dimethylphenyl methyl ether (135630-63-6)

Guidance literature:

3-iodo-2,6-dimethylaniline hydrochloride; With acetic acid; isopentyl nitrite; In 1,4-dioxane; at -5 - 0 ℃; for 2h;

methanol; for 15h; Heating;

DOI:10.1248/cpb.52.1445

upstream raw materials:

1-iodo-2,4-dimethyl-3-nitro-benzene

2,6-dimethylnitrobenzene

Downstream raw materials:

3-iodo-2,6-dimethylphenyl methyl ether

(R)-6,6'-bis(diphenylphosphino)-3,3'-dimethoxy-2,2',4,4'-tetramethyl-1,1'-biphenyl

(R)-6,6'-bis(diphenylphosphoryl)-3,3'-dimethoxy-2,2',4,4'-tetramethyl-1,1'-biphenyl

6,6'-Bis(dicyclohexylphosphino)-3,3'-dimethoxy-2,2',4,4'-tetramethyl-1,1'-biphenyl

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