4H-1-Benzopyran-4-one, 7-hydroxy-5-methoxy-2-(4-methoxyphenyl)-

Base Information

Chemical Name:4H-1-Benzopyran-4-one, 7-hydroxy-5-methoxy-2-(4-methoxyphenyl)-
CAS No.:13698-23-2
Molecular Formula:C17H14O5
Molecular Weight:298.295
Hs Code.:
DSSTox Substance ID:DTXSID80425156
Nikkaji Number:J2.552.919G
Mol file:13698-23-2.mol

Synonyms:13698-23-2;7-hydroxy-5-methoxy-2-(4-methoxyphenyl)-4H-chromen-4-one;SPBio_000930;7-hydroxy-5-methoxy-2-(4-methoxyphenyl)chromen-4-one;Acacetin 5-methyl ether;4H-1-Benzopyran-4-one, 7-hydroxy-5-methoxy-2-(4-methoxyphenyl)-;Spectrum2_000795;BSPBio_002840;SCHEMBL4279323;7-hydroxy-5,4'-dimethoxyflavone;DTXSID80425156;CHEBI:193401;CCG-40173;NCGC00178441-01

Suppliers and Price of 4H-1-Benzopyran-4-one, 7-hydroxy-5-methoxy-2-(4-methoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4H-1-Benzopyran-4-one, 7-hydroxy-5-methoxy-2-(4-methoxyphenyl)-

Chemical Property:

XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:298.08412354
Heavy Atom Count:22
Complexity:438

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=CC(=O)C3=C(O2)C=C(C=C3OC)O

Technology Process of 4H-1-Benzopyran-4-one, 7-hydroxy-5-methoxy-2-(4-methoxyphenyl)-

There total 14 articles about 4H-1-Benzopyran-4-one, 7-hydroxy-5-methoxy-2-(4-methoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 77-78-1
dimethyl sulfate

: 17306-46-6
rhoifolin

: 13698-23-2
apigenin 4',5-dimethyl ether

Guidance literature:: dimethyl sulfate; rhoifolin; In acetone; for 6h;

With sulfuric acid; In ethanol; for 4h; Reflux;
DOI:10.1007/s00044-017-1871-4

Reference yield:

: 111922-60-2
7-O-benzyl-5-O-methylacacetin

: 13698-23-2
apigenin 4',5-dimethyl ether

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 5h; Ambient temperature;

Reference yield:

: 39548-89-5
1-(4-(benzyloxy)-2-hydroxy-6-methoxyphenyl)ethan-1-one

: 13698-23-2
apigenin 4',5-dimethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 350 mg / ethanol; aq. NaOH / 80 h / Ambient temperature

2: 200 mg / SeO₂ / pentan-1-ol

3: 110 mg / H₂ / 10 percent Pd-C / ethyl acetate / 5 h

With selenium(IV) oxide; hydrogen; palladium on activated charcoal; In sodium hydroxide; ethanol; pentan-1-ol; ethyl acetate;