4H-Pyrazolo[3,4-d]pyrimidin-4-one, 5-(4-chlorophenyl)-6-[[2-(dimethylamino)ethyl]thio]-2,5-dihydro-2-(phenyl methyl)-

Base Information

Chemical Name:4H-Pyrazolo[3,4-d]pyrimidin-4-one, 5-(4-chlorophenyl)-6-[[2-(dimethylamino)ethyl]thio]-2,5-dihydro-2-(phenyl methyl)-
CAS No.:136993-42-5
Molecular Formula:C₂₂H₂₂ClN₅OS
Molecular Weight:439.969
Hs Code.:
Mol file:136993-42-5.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4H-Pyrazolo[3,4-d]pyrimidin-4-one, 5-(4-chlorophenyl)-6-[[2-(dimethylamino)ethyl]thio]-2,5-dihydro-2-(phenyl methyl)-

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Technology Process of 4H-Pyrazolo[3,4-d]pyrimidin-4-one, 5-(4-chlorophenyl)-6-[[2-(dimethylamino)ethyl]thio]-2,5-dihydro-2-(phenyl methyl)-

There total 6 articles about 4H-Pyrazolo[3,4-d]pyrimidin-4-one, 5-(4-chlorophenyl)-6-[[2-(dimethylamino)ethyl]thio]-2,5-dihydro-2-(phenyl methyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 136993-33-4
2-Benzyl-5-(4-chloro-phenyl)-6-thioxo-2,5,6,7-tetrahydro-pyrazolo[3,4-d]pyrimidin-4-one

: 107-99-3
2-(dimethylamino)ethyl chloride

: 136993-42-5
2-Benzyl-5-(4-chloro-phenyl)-6-(2-dimethylamino-ethylsulfanyl)-2,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Guidance literature:: With potassium carbonate; In acetone; for 8h; Heating;

Reference yield:

: 21377-11-7
3-Amino-1-benzylpyrazol-4-carbonsaeureethylester

: 136993-42-5
2-Benzyl-5-(4-chloro-phenyl)-6-(2-dimethylamino-ethylsulfanyl)-2,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / acetonitrile / 6 h / Heating

2: 75 percent / methanol. NaOH / 4 h / Heating

3: 45 percent / K₂CO₃ / acetone / 8 h / Heating

With sodium hydroxide; potassium carbonate; In acetone; acetonitrile;

Reference yield:

: 106-47-8
4-chloro-aniline

: 136993-42-5
2-Benzyl-5-(4-chloro-phenyl)-6-(2-dimethylamino-ethylsulfanyl)-2,5-dihydro-pyrazolo[3,4-d]pyrimidin-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / acetonitrile / 6 h / Heating

2: 75 percent / methanol. NaOH / 4 h / Heating

3: 45 percent / K₂CO₃ / acetone / 8 h / Heating

With sodium hydroxide; potassium carbonate; In acetone; acetonitrile;