Cyclohexyldithiocarbamic acid sodium salt

Base Information

• Chemical Name: Cyclohexyldithiocarbamic acid sodium salt
• CAS No.: 2801-07-2
• Molecular Formula: C7H13NS2
• Molecular Weight: 197.301
• Hs Code.: 2930909090
• Mol file: 2801-07-2.mol

Synonyms:monocyclohexyldithiocarbamate sodium;cyclohexyl-dithiocarbamic acid Na salt;Natrium-N-cyclohexyl-dithiocarbamat;sodium N-cyclohexyl dithiocarbamate;

Chemical Property of Cyclohexyldithiocarbamic acid sodium salt

Chemical Property:

• Vapor Pressure: 0.028mmHg at 25°C
• Boiling Point: 245.9°Cat760mmHg
• Flash Point: 102.5°C
• PSA: 82.92000
• Density: 1.13g/cm³
• LogP: 2.51430

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Cyclohexyldithiocarbamic acid sodium salt

There total 2 articles about Cyclohexyldithiocarbamic acid sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

carbon disulfide (75-15-0,12122-00-8) + cyclohexylamine (108-91-8,157973-60-9) → monocyclohexyldithiocarbamate sodium (2801-07-2)

Guidance literature:

With sodium hydroxide; In methanol; diethyl ether; at 20 ℃; for 24h;

DOI:10.1002/ejoc.202100124

Reference yield:

→ monocyclohexyldithiocarbamate sodium (2801-07-2)

Guidance literature:

Reference yield: 76.0%

monocyclohexyldithiocarbamate sodium (2801-07-2) + 2-ethoxycarbonylbenzyl bromide (7115-91-5) → 8-cyclohexyl-7-thioxo-7,8-dihydro-5H-6-thia-8-azabenzocyclohepten-9-one

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1002/jhet.3794

upstream raw materials:

carbon disulfide

cyclohexylamine

Downstream raw materials:

3-cyclohexylamino-4-phenyl-cyclobut-3-ene-1,2-dione

Cyclohexyl-dithiocarbamic acid 3,4-dioxo-2-phenyl-cyclobut-1-enyl ester

In(C₆H₁₁NHCS₂)3

C₅H₅Ni(P(C₄H₉-n)3)SC(S)NHC₆H₁₁-cyclo

Refernces

• 1、 Asgari, Mohammad Sadegh,Bahadorikhalili, Saeed,Asadi, Mehdi,Rashidi Ranjbar, Parviz,Larijani, Bagher,Rahimi, Rahmatollah,Mahdavi, Mohammad. "Amine-carbon disulfide promoted synthesis of novel benzo[e][1,3]thiazepin-5(1H)-one derivatives". . p. 413 - 418. Retrieved 2019/12/24.
• 2、 Alagarsamy, Veerachamy,Solomon, Viswas Raja,Krishnamoorthy,Sulthana,Narendar. "Syntheses and antimicrobial activities of 1-(3-benzyl-4-oxo-3,4-dihydroquinazolin-2-yl)-4-(substituted) thiosemicarbazide derivatives". . p. 1471 - 1479. Retrieved 2016/02/18.