Carbamimidothioic acid,N'-cyano-N-(phenylmethyl)-N-[(trimethylsilyl)methyl]-, methyl ester

Base Information

• Chemical Name: Carbamimidothioic acid,N'-cyano-N-(phenylmethyl)-N-[(trimethylsilyl)methyl]-, methyl ester
• CAS No.: 137777-77-6
• Molecular Formula: C14H21N3SSi
• Molecular Weight: 291.492

Synonyms:Carbamimidothioic acid,N'-cyano-N-(phenylmethyl)-N-[(trimethylsilyl)methyl]-, methyl ester

Chemical Property of Carbamimidothioic acid,N'-cyano-N-(phenylmethyl)-N-[(trimethylsilyl)methyl]-, methyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamimidothioic acid,N'-cyano-N-(phenylmethyl)-N-[(trimethylsilyl)methyl]-, methyl ester

There total 2 articles about Carbamimidothioic acid,N'-cyano-N-(phenylmethyl)-N-[(trimethylsilyl)methyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-cyano-N'-trimethylsilylmethyl-S-methylisothiourea (137777-74-3) → N-cyano-N'-benzyl-N'-trimethylsilylmethyl-S-methylisothiourea (137777-77-6)

Guidance literature:

With potassium carbonate; In acetone; Ambient temperature;

DOI:10.1016/S0040-4039(00)79445-7

Reference yield: 93.0%

benzyl bromide (100-39-0) + N-cyano-N'-trimethylsilylmethyl-S-methylisothiourea (137777-74-3) → N-cyano-N'-benzyl-N'-trimethylsilylmethyl-S-methylisothiourea (137777-77-6)

Guidance literature:

With potassium carbonate; In acetone; for 48h; Ambient temperature;

DOI:10.1248/cpb.43.1425

Reference yield: 66.0%

benzaldehyde (100-52-7) + N-cyano-N'-benzyl-N'-trimethylsilylmethyl-S-methylisothiourea (137777-77-6) → 3-benzyl-2-cyanoimino-4,5-dihydro-5-phenyl-1,3-oxazole (137777-94-7)

Guidance literature:

With cesium fluoride; In acetonitrile; Ambient temperature;

DOI:10.1016/S0040-4039(00)79445-7

upstream raw materials:

benzyl bromide

N-cyano-N'-trimethylsilylmethyl-S-methylisothiourea

Downstream raw materials:

3-benzyl-2-cyanoimino-4,5-dihydro-1-methyl-5,5-diphenyl-1,3-oxazole

3-benzyl-2-cyanoimino-4,5-dihydro-5-phenyl-1,3-oxazole

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