Ethanedione, bis[3,4-bis(hexyloxy)phenyl]-

Base Information

Chemical Name:Ethanedione, bis[3,4-bis(hexyloxy)phenyl]-
CAS No.:138145-24-1
Molecular Formula:C38H58O6
Molecular Weight:610.875
Hs Code.:
DSSTox Substance ID:DTXSID10438431
Nikkaji Number:J568.793D
Wikidata:Q82254176
Mol file:138145-24-1.mol

Synonyms:Ethanedione, bis[3,4-bis(hexyloxy)phenyl]-;138145-24-1;DTXSID10438431;1,2-Bis[3,4-bis(hexyloxy)phenyl]-1,2-ethanedione

Suppliers and Price of Ethanedione, bis[3,4-bis(hexyloxy)phenyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Ethanedione, bis[3,4-bis(hexyloxy)phenyl]-

Chemical Property:

XLogP3:12.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:27
Exact Mass:610.42333957
Heavy Atom Count:44
Complexity:666

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCOC1=C(C=C(C=C1)C(=O)C(=O)C2=CC(=C(C=C2)OCCCCCC)OCCCCCC)OCCCCCC

Technology Process of Ethanedione, bis[3,4-bis(hexyloxy)phenyl]-

There total 4 articles about Ethanedione, bis[3,4-bis(hexyloxy)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 111-25-1
1-bromo-hexane

: 6309-15-5
3,3',4,4'-tetrahydroxybenzil

: 138145-24-1
1,2-bis(3,4-bis(hexyloxy)phenyl)ethane-1,2-dione

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1039/b400998c

Reference yield: 79.0%

: 79-37-8
oxalyl dichloride

: 94259-20-8
1,2-dihexyloxybenzene

: 138145-24-1
1,2-bis(3,4-bis(hexyloxy)phenyl)ethane-1,2-dione

Guidance literature:: With aluminum (III) chloride; at 0 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1039/c8ta04774j

Reference yield:

: 111-25-1
1-bromo-hexane

: 138145-24-1
1,2-bis(3,4-bis(hexyloxy)phenyl)ethane-1,2-dione

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 9 h / 80 °C

2: 24 percent / AlCl₃ / CS₂ / 18 h / 0 °C

With aluminium trichloride; potassium carbonate; In carbon disulfide; N,N-dimethyl-formamide;
DOI:10.1021/jo00082a022