1-[(Phenylsulfanyl)methyl]-2-naphthol

Base Information

Chemical Name:1-[(Phenylsulfanyl)methyl]-2-naphthol
CAS No.:72862-46-5
Molecular Formula:C17H14OS
Molecular Weight:266.364
Hs Code.:
NSC Number:89492
DSSTox Substance ID:DTXSID80293438
Wikidata:Q82032164

Synonyms:72862-46-5;1-[(phenylsulfanyl)methyl]-2-naphthol;NSC89492;DTXSID80293438;NSC-89492

Suppliers and Price of 1-[(Phenylsulfanyl)methyl]-2-naphthol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-[(Phenylsulfanyl)methyl]-2-naphthol

Chemical Property:

Vapor Pressure:4.64E-09mmHg at 25°C
Boiling Point:459.4°Cat760mmHg
Flash Point:222.9°C
Density:1.25g/cm³
XLogP3:4.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:266.07653624
Heavy Atom Count:19
Complexity:274

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)SCC2=C(C=CC3=CC=CC=C32)O

Technology Process of 1-[(Phenylsulfanyl)methyl]-2-naphthol

There total 7 articles about 1-[(Phenylsulfanyl)methyl]-2-naphthol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1354018-46-4
(2-[(tert-butyldimethylsilyl)oxy]-1-naphthyl)methyl nitrate

: 108-98-5
thiophenol

: 72862-46-5
1-[(phenylthio)methyl]naphthalen-2-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 - 20 ℃; for 0.2h; Inert atmosphere;
DOI:10.1021/ol203196n

Reference yield: 68.0%

: 108-98-5
thiophenol

: 28918-29-8
1-((1H-benzotriazol-1-yl)methyl)naphthalen-2-ol

: 72862-46-5
1-[(phenylthio)methyl]naphthalen-2-ol

Guidance literature:: With sodium isopropylate; In isopropyl alcohol; for 20h; Heating;
DOI:10.1021/jo00086a050

Reference yield:

: 1354018-42-0
{2-[(tert-butyldimethylsilyl)oxy]naphthalen-1-yl}methanol

: 72862-46-5
1-[(phenylthio)methyl]naphthalen-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride; silver nitrate / tetrahydrofuran / 25 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.2 h / -78 - 20 °C / Inert atmosphere

With thionyl chloride; tetrabutyl ammonium fluoride; silver nitrate; In tetrahydrofuran;
DOI:10.1021/ol203196n