1,3,4-Trimethylpyridinium iodide

Base Information

• Chemical Name: 1,3,4-Trimethylpyridinium iodide
• CAS No.: 6283-41-6
• Molecular Formula: C8H12N+
• Molecular Weight: 249.094
• DSSTox Substance ID: DTXSID40501945
• NSC Number: 7493

Synonyms:1,3,4-trimethylpyridinium iodide;6283-41-6;1,3,4-trimethyl-pyridinium iodide;1,3,4-Trimethyl-pyridinium;iodide;SCHEMBL3857270;DTXSID40501945;NSC7493;LNUYBCUFHJCJFD-UHFFFAOYSA-M;NSC-7493;1,3,4-Trimethylpyridin-1-ium iodide;1,3,4-trimethylpyridin-1-ium;AKOS024388294

Chemical Property of 1,3,4-Trimethylpyridinium iodide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: g/cm³
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 249.00145
• Heavy Atom Count: 10
• Complexity: 90.6

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC1=C(C=[N+](C=C1)C)C.[I-]

Technology Process of 1,3,4-Trimethylpyridinium iodide

There total 1 articles about 1,3,4-Trimethylpyridinium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3,4-Lutidin (583-58-4) + methyl iodide (74-88-4) → 1,3,4-trimethylpyridinium iodide (6283-41-6)

Guidance literature:

In diethyl ether; at 20 ℃; for 120h;

DOI:10.1002/1099-0690(200006)2000:11<2013::AID-EJOC2013>3.0.CO;2-A

Reference yield:

4-methoxybenzylmagnesium chloride (38769-92-5) + 1,3,4-trimethylpyridinium iodide (6283-41-6) → (+/-)-3,6,11syn-trimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-benz[d]azocin-8-ol (3734-52-9,21286-57-7,21286-60-2,25144-79-0,25145-09-9,58640-79-2,64023-94-5,67009-58-9,69831-04-5,36402-80-9,75257-89-5,1509-00-8)

Guidance literature:

With diethyl ether; Hydrieren des nach der Hydrolyse erhaltenen Reaktionsprodukts an Palladium/Bariumsulfat in wss. Salzsaeure und Erhitzen des Hydrierungsprodukts mit wss. Bromwasserstoffsaeure auf 135-140grad.;

DOI:10.1021/jo01362a017 DOI:10.1021/jo01092a011

Reference yield:

4-methoxybenzylmagnesium chloride (38769-92-5) + 1,3,4-trimethylpyridinium iodide (6283-41-6) → (+/-)-3,6,11anti-trimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-benz[d]azocin-8-ol (3734-52-9,21286-57-7,21286-60-2,25144-79-0,25145-09-9,58640-79-2,64023-94-5,67009-58-9,69831-04-5,36402-80-9,75257-89-5,1509-00-8)

Guidance literature:

With diethyl ether; Hydrieren des nach der Hydrolyse erhaltenen Reaktionsprodukts an Palladium/Bariumsulfat in wss. Salzsaeure und Erhitzen des Hydrierungsprodukts mit wss. Bromwasserstoffsaeure auf 135-140grad.;

DOI:10.1021/jo01362a017 DOI:10.1021/jo01092a011

upstream raw materials:

3,4-Lutidin

methyl iodide

Downstream raw materials:

4-(1,3,4-Trimethyl-[2]piperidylmethyl)-phenol

(+/-)-3,6,11syn-trimethyl-1,2,3,4,5,6-hexahydro-2,6-methano-benz[d]azocine

Tetrahydropyridin

1,4,5-Trimethyl-6-(4-methylsulfanyl-benzyl)-1,2,3,6-tetrahydro-pyridine

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