4-morpholinocyclohexanone

Base Information

Chemical Name:4-morpholinocyclohexanone
CAS No.:139025-93-7
Molecular Formula:C10H17NO2
Molecular Weight:183.25
Hs Code.:2934999090
Mol file:139025-93-7.mol

Synonyms:4-(morpholin-4-yl)cyclohexan-1-one;4-morpholin-4-yl-cyclohexanone;4-morpholinocyclohexanone;

Suppliers and Price of 4-morpholinocyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
4-(Morpholin-4-yl)cyclohexanone
100mg
$ 150.00

Medical Isotopes, Inc.
4-(Morpholin-4-yl)cyclohexanone
100 mg
$ 650.00

Matrix Scientific
4-Morpholinocyclohexanone 95+%
250mg
$ 445.00

Matrix Scientific
4-Morpholinocyclohexanone 95+%
1g
$ 958.00

Crysdot
4-Morpholinocyclohexanone 95+%
5g
$ 978.00

Crysdot
4-Morpholinocyclohexanone 95+%
1g
$ 285.00

Chemenu
4-morpholinocyclohexan-1-one 95%
1g
$ 355.00

American Custom Chemicals Corporation
4-MORPHOLINOCYCLOHEXANONE 95.00%
1G
$ 1630.86

Ambeed
4-Morpholinocyclohexanone 95%
250mg
$ 67.00

Ambeed
4-Morpholinocyclohexanone 95%
100mg
$ 33.00

Total 24 raw suppliers

Chemical Property of 4-morpholinocyclohexanone

Chemical Property:

PSA：29.54000
LogP:0.76820
Storage Temp.:2-8°C
Solubility.:Chloroform (Slightly), DMSO (Slightly), Ethyl Acetate (Slightly), Methanol (Slig

Purity/Quality:

97% ^*data from raw suppliers

4-(Morpholin-4-yl)cyclohexanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 4-(Morpholin-4-yl)cyclohexanone is a useful synthetic intermediate. It was used to synthesize diastereomeric 3,6-diaminobicyclo[3.1.0]hexane derivatives.

Technology Process of 4-morpholinocyclohexanone

There total 3 articles about 4-morpholinocyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 127562-53-2
4-(1,4-dioxaspiro<4.5>dec-8-yl)morpholine

: 139025-93-7
4-(morpholin-4-yl)cyclohexan-1-one

Guidance literature:: 4-(1,4-dioxaspiro<4.5>dec-8-yl)morpholine; With hydrogenchloride; water; In tetrahydrofuran; for 17h;

With water; sodium hydrogencarbonate; In tetrahydrofuran;

Reference yield: 47.0%

: 954135-73-0
4-(1,4-dioxa-spiro[4.5]dec-8-yl)-morpholine hydrochloride

: 139025-93-7
4-(morpholin-4-yl)cyclohexan-1-one

Guidance literature:: 4-(1,4-dioxa-spiro[4.5]dec-8-yl)-morpholine hydrochloride; With hydrogenchloride; In tetrahydrofuran; water; at 80 ℃; for 4h;

With sodium hydrogencarbonate; In tetrahydrofuran; water; pH=7;

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 139025-93-7
4-(morpholin-4-yl)cyclohexan-1-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1) titanium isopropoxide, 2) sodium cyanoborohydride / 1) 1 h, r.t., 2) EtOH, 24 h, r.t.

2: 59 percent / 12.5 N HCl, water / 96 h / Ambient temperature

With titanium(IV) isopropylate; hydrogenchloride; water; sodium cyanoborohydride;
DOI:10.1055/s-1991-28406