N-(4-methoxyphenyl)benzenesulfonamide

Base Information

• Chemical Name: N-(4-methoxyphenyl)benzenesulfonamide
• CAS No.: 7471-26-3
• Molecular Formula: C13H13NO3S
• Molecular Weight: 263.317
• Hs Code.: 2935009090
• Mol file: 7471-26-3.mol

Synonyms:benzenesulfonic acid p-anisidide;Benzolsulfonsaeure-p-anisidid;JUEQLTHFAHLSAQ-UHFFFAOYSA;N-(4-methoxyphenyl)-4-fluorobenzamide;N-4-methoxyphenylbenzenesulfonamide;N-(p-anisyl)-4-fluorobenzamide;Benzamide,N-(4-methoxyphenyl)-4-fluoro;

Chemical Property of N-(4-methoxyphenyl)benzenesulfonamide

Chemical Property:

• Melting Point: 88-89 °C
• Boiling Point: 417.8°Cat760mmHg
• PKA: 9.39±0.10(Predicted)
• Flash Point: 206.5°C
• PSA: 63.78000
• Density: 1.299g/cm³
• LogP: 3.64980

Purity/Quality:

97% ^*data from raw suppliers

N-(4-Methoxyphenyl)benzenesulfonamide 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-methoxyphenyl)benzenesulfonamide

There total 36 articles about N-(4-methoxyphenyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-[2-chloro-1-(4-methoxyphenyl)ethyl]-N-fluorobenzenesulfonamide → 2-chloroethanal (107-20-0) + N-(4-methoxyphenyl)benzenesulphonamide (7471-26-3)

Guidance literature:

With formic acid; at 50 ℃;

DOI:10.1021/acs.joc.8b01841

Reference yield: 94.0%

benzenesulfonamide (98-10-2) + 1-bromo-4-methoxy-benzene (104-92-7) → N-(4-methoxyphenyl)benzenesulphonamide (7471-26-3)

Guidance literature:

With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine; In acetonitrile; at 70 ℃; for 8h; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.10.113

Reference yield: 94.0%

para-methoxynitrobenzene (100-17-4) + benzenesulfonyl chloride (98-09-9) → N-(4-methoxyphenyl)benzenesulphonamide (7471-26-3)

Guidance literature:

With iron; In water; for 0.833333h;

upstream raw materials:

4-benzenesulfonylamino-benzenediazonium-betaine

4-methoxy-aniline

benzenesulfonyl chloride

N-(phenylsulfonyl)-1,4-benzoquinone monoimine

Downstream raw materials:

N-(4-methoxy-2-nitrophenyl)benzenesulfonamide

N-benzenesulfonyl-N-acetyl-p-anisidide

N-(4-Ethoxy-4-methoxy-cyclohexa-2,5-dienylidene)-benzenesulfonamide

p-benzoquinone