BenzeneMethanol,3,4-diMethyl-α-phenyl-

Base Information

• Chemical Name: BenzeneMethanol,3,4-diMethyl-α-phenyl-
• CAS No.: 14189-53-8
• Molecular Formula: C15H16O
• Molecular Weight: 212.291
• Mol file: 14189-53-8.mol

Synonyms:4-Aethyl-mandelsaeure;p-Aethylphenylglyoxylsaeure;3,4-Dimethyl-benzhydrol;4-ethyl-mandelic acid;p-Ethyl-mandelsaeure;p-Aethyl-mandelsaeure;

Chemical Property of BenzeneMethanol,3,4-diMethyl-α-phenyl-

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 63.0-63.6 °C
• Boiling Point: 354.023oC at 760 mmHg
• PKA: 13.83±0.20(Predicted)
• Flash Point: 149.952oC
• PSA: 20.23000
• Density: 1.063g/cm3
• LogP: 3.38510

Purity/Quality:

99.90% ^*data from raw suppliers

(3,4-DIMETHYLPHENYL)(PHENYL)METHANOL ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BenzeneMethanol,3,4-diMethyl-α-phenyl-

There total 7 articles about BenzeneMethanol,3,4-diMethyl-α-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(3,4-dimethylphenyl)(phenyl)methanone (2571-39-3) → 3,4-dimethylbenzhydrol (14189-53-8)

Guidance literature:

With palladium; hydrogen; In acetone; at 50 ℃; for 22h;

Reference yield: 54.0%

bromobenzene (108-86-1,52753-63-6) + 3,4-dimethylbenzaldehyde (5973-71-7) → 3,4-dimethylbenzhydrol (14189-53-8)

Guidance literature:

bromobenzene; With iodine; magnesium; In diethyl ether; at 0 ℃; for 0.166667h;

3,4-dimethylbenzaldehyde; In diethyl ether; for 12h;

DOI:10.1016/j.tetlet.2013.01.088

Reference yield:

4-bromo-o-xylene (583-71-1) + benzaldehyde (100-52-7) → 3,4-dimethylbenzhydrol (14189-53-8)

Guidance literature:

4-bromo-o-xylene; benzaldehyde; With magnesium; In tetrahydrofuran; at 20 - 85 ℃; for 2h;

In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol302181z

upstream raw materials:

(3,4-dimethylphenyl)(phenyl)methanone

o-xylene

benzoyl chloride

2-(3,4-dimethylbenzoyl)benzoic acid

Downstream raw materials:

4-benzyl-1,2-dimethylbenzene

3-((3,4-dimethylphenyl)(phenyl)methyl)-4-hydroxy-2H-chromen-2-one

ethyl 2-((3,4-dimethylphenyl)(phenyl)methyl)-3-oxobutanoate

3-((3,4-dimethylphenyl)(phenyl)methyl)pentane-2,4-dione