Technology Process of Sapintoxin d
There total 4 articles about Sapintoxin d which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine
2: DCC / DMAP / dimethylformamide
3: 1.) 1percent HClO4, 2.) piperidine / 1.) MeOH, 24 h, 2.) CH2Cl2
With
piperidine; pyridine; perchloric acid; dicyclohexyl-carbodiimide;
dmap;
In
N,N-dimethyl-formamide;
DOI:10.1016/0031-9422(88)80229-2
- Guidance literature:
-
Multi-step reaction with 2 steps
1: DCC / DMAP / dimethylformamide
2: 1.) 1percent HClO4, 2.) piperidine / 1.) MeOH, 24 h, 2.) CH2Cl2
With
piperidine; perchloric acid; dicyclohexyl-carbodiimide;
dmap;
In
N,N-dimethyl-formamide;
DOI:10.1016/0031-9422(88)80229-2
- Guidance literature:
-
Multi-step reaction with 2 steps
1: DCC / DMAP / dimethylformamide
2: 1.) 1percent HClO4, 2.) piperidine / 1.) MeOH, 24 h, 2.) CH2Cl2
With
piperidine; perchloric acid; dicyclohexyl-carbodiimide;
dmap;
In
N,N-dimethyl-formamide;
DOI:10.1016/0031-9422(88)80229-2