Phenyl(2,4,6-trimethylphenyl)phosphinic acid

Base Information

Chemical Name:Phenyl(2,4,6-trimethylphenyl)phosphinic acid
CAS No.:142087-69-2
Molecular Formula:C15H17O2P
Molecular Weight:260.273
Hs Code.:
DSSTox Substance ID:DTXSID00569142
Wikidata:Q82456223

Synonyms:142087-69-2;Phenyl(2,4,6-trimethylphenyl)phosphinic acid;SCHEMBL15717372;DTXSID00569142

Suppliers and Price of Phenyl(2,4,6-trimethylphenyl)phosphinic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Phenyl(2,4,6-trimethylphenyl)phosphinic acid

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:260.09661678
Heavy Atom Count:18
Complexity:311

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)P(=O)(C2=CC=CC=C2)O)C

Technology Process of Phenyl(2,4,6-trimethylphenyl)phosphinic acid

There total 5 articles about Phenyl(2,4,6-trimethylphenyl)phosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: phenyl-(2,4,6-trimethylphenyl)phosphinic acid ethyl ester

: 142087-69-2
P-phenyl-P-2,4,6-trimethylphenylphosphinic acid

Guidance literature:: With water; sodium hydroxide; at 80 ℃;
DOI:10.1021/jo401608v

Reference yield:

: C₁₉H₂₆NOP

: 142087-69-2
P-phenyl-P-2,4,6-trimethylphenylphosphinic acid

Guidance literature:: With hydrogenchloride; In acetone; for 144h; Yield given; Ambient temperature;

Reference yield:

: 644-97-3
Dichlorophenylphosphine

: 142087-69-2
P-phenyl-P-2,4,6-trimethylphenylphosphinic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / diethyl ether / a) 0 deg C, 2 h, 2.) RT, overnight

2: 1.) Mg, 1,2-dibromoethane / 1.) Et₂O, reflux, 3 h, 2.) Et₂O, a) 0 deg C, 5 h, b) RT, overnight

3: 15percent H₂O₂ / acetone / 4 h / Heating

4: conc. HCl / acetone / 144 h / Ambient temperature

With hydrogenchloride; dihydrogen peroxide; magnesium; ethylene dibromide; In diethyl ether; acetone;