Technology Process of Stannane, bis(2,6-dimethoxyphenyl)dimethyl-
There total 3 articles about Stannane, bis(2,6-dimethoxyphenyl)dimethyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
diethyl ether;
suspension of Li-compd. (prepared form C6H4(OCH3)2, 15% hexane soln. of BuLi and TMEDA under Ar, at room temp for 1-2) added to suspension of Sn-compd. under Ar, stirred at room temp. for 3 h; washed (H2O), concd. (vac.), recrystd. (hexane or MeOH); elem. anal.;
DOI:10.1246/bcsj.65.1389
- Guidance literature:
-
In
diethyl ether;
suspension of Li-compd. (prepared form C6H4(OCH3)2, 15% hexane soln. of BuLi and TMEDA under Ar, at room temp for 1-2) added to suspension of Sn-compd. under Ar, stirred at room temp. for 5 h; washed (H2O), evapd. (vac.), recrystd. (MeOH);
DOI:10.1246/bcsj.65.1389
- Guidance literature:
-
In
not given;
deprotonation of 1,3-dimethoxybenzene followed by quenching with Sn compd.;
DOI:10.1021/ic034150x
