Technology Process of Acetamide,
N-(5,6-dihydro-5-methyl-6-oxo-2,2-diphenyl-1,3-dithiino[5,4-b]pyrrol-7-yl
)-
There total 10 articles about Acetamide,
N-(5,6-dihydro-5-methyl-6-oxo-2,2-diphenyl-1,3-dithiino[5,4-b]pyrrol-7-yl
)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trichlorophosphate;
In
tetrahydrofuran;
for 1h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 10 steps
1: 90 percent / AlCl3 / CH2Cl2 / 1 h / Ambient temperature
2: 80 percent / NaOMe / methanol; diethyl ether / 48 h / Ambient temperature
3: 100 percent / N-methylmorpholine / benzene / 12 h
4: 90 percent / 2 N H2SO4 / 8 h / Heating
5: acetonitrile; ethanol / 48 h / Ambient temperature
6: 71 percent / KOH / methanol / 12 h / Ambient temperature
7: 60 percent / TsCl, Et3N / toluene / 2 h / Heating
8: 70 percent / AlCl3 / 1 h / Ambient temperature
9: 90 percent / NH2OH*HCl / methanol / 24 h / 60 °C
10: 65 percent / POCl3 / tetrahydrofuran / 1 h / Ambient temperature
With
4-methyl-morpholine; potassium hydroxide; aluminium trichloride; sulfuric acid; hydroxylamine hydrochloride; sodium methylate; triethylamine; p-toluenesulfonyl chloride; trichlorophosphate;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; benzene;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / AlCl3 / 1 h / Ambient temperature
2: 90 percent / NH2OH*HCl / methanol / 24 h / 60 °C
3: 65 percent / POCl3 / tetrahydrofuran / 1 h / Ambient temperature
With
aluminium trichloride; hydroxylamine hydrochloride; trichlorophosphate;
In
tetrahydrofuran; methanol;
