1,1,1,3-Tetrachloro-3,3-difluoropropane

Base Information

• Chemical Name: 1,1,1,3-Tetrachloro-3,3-difluoropropane
• CAS No.: 460-89-9
• Molecular Formula: C3H2 Cl4 F2
• Molecular Weight: 217.858
• Hs Code.: 2903791090
• DSSTox Substance ID: DTXSID10196685
• Nikkaji Number: J1.149.497H
• Wikidata: Q83069707
• Mol file: 460-89-9.mol

Synonyms:1,1,1,3-Tetrachloro-3,3-difluoropropane;460-89-9;HCFC 232;HCFC-232fb;C3H2Cl4F2;SCHEMBL7205228;DTXSID10196685;Propane, 1,1,1,3-tetrachloro-3,3-difluoro-

Chemical Property of 1,1,1,3-Tetrachloro-3,3-difluoropropane

Chemical Property:

• Vapor Pressure: 9.38mmHg at 25°C
• Boiling Point: 135.8°Cat760mmHg
• Flash Point: 41.9°C
• PSA: 0.00000
• Density: 1.618g/cm³
• LogP: 3.57830
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 217.884917
• Heavy Atom Count: 9
• Complexity: 96.5

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(C(F)(F)Cl)C(Cl)(Cl)Cl

Technology Process of 1,1,1,3-Tetrachloro-3,3-difluoropropane

There total 2 articles about 1,1,1,3-Tetrachloro-3,3-difluoropropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetrachloromethane (56-23-5) + Vinylidene fluoride (75-38-7) → 1,1,1,3-tetrachloro-3,3-difluoro-propane (460-89-9) + 1,1,1,5-Tetrachloro-3,3,5,5-tetrafluoro-pentane (76140-27-7) + 1,1,1,7-Tetrachloro-3,3,5,5,7,7-hexafluoro-heptane (76140-28-8)

Guidance literature:

di-tert-butyl peroxide; at 130 ℃; for 5h; under 18751.5 Torr;

DOI:10.1016/S0022-1139(00)80451-0

Reference yield:

1,1,3-trichloro-3,3-difluoropropane (460-63-9) → 1,1,1,3-tetrachloro-3,3-difluoro-propane (460-89-9)

Guidance literature:

beim Chlorieren;

Reference yield:

1,1,1,3-tetrachloro-3,3-difluoro-propane (460-89-9) → 1,1,1,3,3,3-hexafluoropropane (690-39-1)

Guidance literature:

bei der Einw_.von fluorierenden Mitteln;

upstream raw materials:

1,1,3-trichloro-3,3-difluoropropane

tetrachloromethane

Vinylidene fluoride

Downstream raw materials:

1,1,1,3,3,3-hexafluoropropane