Silane, [4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]trimethyl-

Base Information

• Chemical Name: Silane, [4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]trimethyl-
• CAS No.: 143106-12-1
• Molecular Formula: C15H28OSi2
• Molecular Weight: 280.558
• DSSTox Substance ID: DTXSID70474193
• Nikkaji Number: J501.638J
• Wikidata: Q82304032

Synonyms:143106-12-1;Silane, [4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]trimethyl-;DTXSID70474193

Chemical Property of Silane, [4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]trimethyl-

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 4
• Exact Mass: 280.16786858
• Heavy Atom Count: 18
• Complexity: 265

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(C)(C)[Si](C)(C)OC1=CC=C(C=C1)[Si](C)(C)C

Technology Process of Silane, [4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]trimethyl-

There total 7 articles about Silane, [4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]phenyl]trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

1-<(tert-butyldimethylsilyl)oxy>-4-chlorobenzene (126644-72-2) + sodium trimethylsilyldimethylsilanolate → tert-butyldimethyl(4-trimethylsilylphenoxy)silane (143106-12-1)

Guidance literature:

With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; Dimethyl(phenyl)phosphine; In toluene; at 70 ℃; for 15h; Schlenk technique; Sealed tube;

DOI:10.1039/d1cc02683f

Reference yield: 74.0%

1-(tert-Butyl-dimethyl-silanyloxy)-4-trimethylsilanyl-cyclohexa-1,4-diene (143106-10-9) → tert-butyldimethyl(4-trimethylsilylphenoxy)silane (143106-12-1)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; or chloranil;

DOI:10.1021/jo00044a008

Reference yield: 73.0%

t-butyldimethylsilyl-4-bromophenol (67963-68-2) + sodium trimethylsilyldimethylsilanolate → tert-butyldimethyl(4-trimethylsilylphenoxy)silane (143106-12-1)

Guidance literature:

With MePhos Pd G₄; In 1,2-dichloro-ethane; at 50 ℃;

DOI:10.1021/acscatal.1c02733

upstream raw materials:

2-(tert-butyldimethylsiloxy)-1,3-butadiene

B-<2-(trimethylsilyl)ethynyl>-9-borabicyclo<3.3.1>nonane*THF

1-(tert-Butyl-dimethyl-silanyloxy)-4-trimethylsilanyl-cyclohexa-1,4-diene

tert-butyldimethylsilyl chloride

Downstream raw materials:

tert-butyldimethyl(phenoxy)silane

4-(trimethylsilyl)phenol

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