6-azido-2-fluoro-7H-purine

Base Information

• Chemical Name: 6-azido-2-fluoro-7H-purine
• CAS No.: 143482-58-0
• Molecular Formula: C5H2FN7
• Molecular Weight: 179.116
• DSSTox Substance ID: DTXSID50600074
• Wikidata: Q82496033

Synonyms:6-azido-2-fluoro-7H-purine;143482-58-0;2-FLUORO-6-AZIDOPURINE;6-azido-2-fluoropurine;DTXSID50600074;OEWGNZVHZJPGGX-UHFFFAOYSA-N

Chemical Property of 6-azido-2-fluoro-7H-purine

Chemical Property:

• XLogP3: 1.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 1
• Exact Mass: 179.03557126
• Heavy Atom Count: 13
• Complexity: 239

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=NC2=C(N1)C(=NC(=N2)F)N=[N+]=[N-]

Technology Process of 6-azido-2-fluoro-7H-purine

There total 1 articles about 6-azido-2-fluoro-7H-purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert.-butylnitrite (540-80-7) + potassium fluoborate (KBF4) + 6-azido-7(9)H-purin-2-ylamine → 6-azido-2-fluoropurine (143482-58-0)

Guidance literature:

In tetrahydrofuran; water;

Reference yield:

2,3,5-tri-O-benzyl-1-(4-nitrobenzoyloxy)-D-arabinofuranose (52522-49-3) + 2,3,5-tri-O-benzyl-α-D-arabinofuranosyl chloride (4060-34-8) + ? molecular sieve + 6-azido-2-fluoropurine (143482-58-0) → Fludarabine (146-78-1,19768-92-4,21679-14-1,21679-15-2)

Guidance literature:

With sodium borohydrid; In methanol; dichloromethane; water; isopropyl alcohol; acetonitrile;

Reference yield:

6-azido-2-fluoropurine (143482-58-0) → 2-fluoroadenine (700-49-2)

Guidance literature:

With sodium borohydrid; In water; isopropyl alcohol;

upstream raw materials:

tert.-butylnitrite

Downstream raw materials:

2-fluoroadenine

Fludarabine

6-azido-2-fluoro-9-(2,3,5-tri-O-benzyl-β-D-arabinofuranosyl)purine

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