Technology Process of Ethyl 2-hydroxy-5-octadecylbenzoate
There total 4 articles about Ethyl 2-hydroxy-5-octadecylbenzoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 86 percent / Zn(Hg), 9 M aq. HCl, glacial acetic acid / toluene / 48 h / Heating
2: 1.) H2SO4, 2.) Br2 / 1.) reflux, 24 h, 2.) CCl4
With
hydrogenchloride; sulfuric acid; bromine; acetic acid; mercury; zinc;
In
toluene;
DOI:10.1021/ja00047a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / AlCl3 / nitrobenzene / 25 °C
2: 86 percent / Zn(Hg), 9 M aq. HCl, glacial acetic acid / toluene / 48 h / Heating
3: 1.) H2SO4, 2.) Br2 / 1.) reflux, 24 h, 2.) CCl4
With
hydrogenchloride; aluminium trichloride; sulfuric acid; bromine; acetic acid; mercury; zinc;
In
nitrobenzene; toluene;
DOI:10.1021/ja00047a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 70 percent / AlCl3 / nitrobenzene / 25 °C
2: 86 percent / Zn(Hg), 9 M aq. HCl, glacial acetic acid / toluene / 48 h / Heating
3: 1.) H2SO4, 2.) Br2 / 1.) reflux, 24 h, 2.) CCl4
With
hydrogenchloride; aluminium trichloride; sulfuric acid; bromine; acetic acid; mercury; zinc;
In
nitrobenzene; toluene;
DOI:10.1021/ja00047a023
