Germane, methyl(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:Germane, methyl(2,4,6-trimethylphenyl)-
CAS No.:143880-60-8
Molecular Formula:C10H16Ge
Molecular Weight:208.827
Hs Code.:

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Chemical Property of Germane, methyl(2,4,6-trimethylphenyl)-

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Technology Process of Germane, methyl(2,4,6-trimethylphenyl)-

There total 3 articles about Germane, methyl(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 143880-59-5
mesityldihydrogermyllithium

: 143880-60-8
((CH₃)3C₆H₂)H₂GeCH₃

Guidance literature:: With methyl iodide; In tetrahydrofuran; byproducts: LiI; under inert atm.; excess of MeI added to MesH2GeLi at -60°C; stirred for 30 min; warmed to room temp.; hydrolyzed; ext. concd. (reduced pressure); distd.; elem.anal.;
DOI:10.1016/0022-328X(92)80129-L

Reference yield: 35.0%

: 72876-20-1
2,4,6-trimethylphenylgermanium trihydride

: 143880-60-8
((CH₃)3C₆H₂)H₂GeCH₃

: 143880-77-7
((CH₃)3C₆H₂)HGe(CH₃)2

Guidance literature:: With tert.-butyl lithium; methyl iodide; In tetrahydrofuran; byproducts: LiI; under inert atm.; dropwise addn. of an excess of t-BuLi (pentane) and MeI to MesGeH3 at -60°C; 40 min at -60°C; warming to 20°C;
DOI:10.1016/0022-328X(92)80129-L

Reference yield: 24.0%

: 72876-20-1
2,4,6-trimethylphenylgermanium trihydride

: 74-88-4
methyl iodide

: 143880-60-8
((CH₃)3C₆H₂)H₂GeCH₃

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; hexane; t-BuLi in hexane was added to soln. of Ge-complex in THF at -50°C, stirred at -50°C for 10 min, MeI was added, 20 min at -50.degre.C, warmed to room temp. under Ar, stirred for 1 h, quenched with HCl; aq. phase was extd. with hexane, dried over MgSO4, solvent was removed in vacuo, distilled at 60°C 2 mmHg; elem. anal.;
DOI:10.1139/v00-058