Eulophiol

Base Information

Chemical Name:Eulophiol
CAS No.:87402-72-0
Molecular Formula:C₁₆H₁₆O₄
Molecular Weight:272.301
Hs Code.:

Synonyms:

Suppliers and Price of Eulophiol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

ChemScene
Eulophiol
5mg
$ 1150.00

Total 10 raw suppliers

Chemical Property of Eulophiol

Chemical Property:

PSA：0.00000
LogP:0.00000

Purity/Quality:

99% ^*data from raw suppliers

Eulophiol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Eulophiol

There total 8 articles about Eulophiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.2%

: 1,5-dibenzyloxy-2,7-dimethoxy-phenanthrene

: 87402-72-0
eulophiol

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; ethyl acetate; for 24h; under 3620.13 Torr;
DOI:10.1016/j.ejmech.2013.06.016

Reference yield:

: 148-53-8
3-methoxy-2-hydroxybenzaldehyde

: 87402-72-0
eulophiol

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C

2.1: sodium tetrahydroborate / isopropyl alcohol / 2 h / Reflux

3.1: phosphorus tribromide / dichloromethane / 1 h / 0 °C

4.1: toluene / 4 h / Reflux

5.1: lithium methanolate / N,N-dimethyl-formamide / 1 h / 100 - 220 °C / Inert atmosphere

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Reflux

6.2: 2 h / Reflux

7.1: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 24 h / 3620.13 Torr

With sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); palladium 10% on activated carbon; lithium methanolate; hydrogen; tri-n-butyl-tin hydride; phosphorus tribromide; potassium carbonate; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 5.1: |Wittig Olefination;
DOI:10.1016/j.ejmech.2013.06.016

Reference yield:

: 2011-06-5
2-benzyloxy-3-methoxybenzaldehyde

: 87402-72-0
eulophiol

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / isopropyl alcohol / 2 h / Reflux

2.1: phosphorus tribromide / dichloromethane / 1 h / 0 °C

3.1: toluene / 4 h / Reflux

4.1: lithium methanolate / N,N-dimethyl-formamide / 1 h / 100 - 220 °C / Inert atmosphere

5.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Reflux

5.2: 2 h / Reflux

6.1: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 24 h / 3620.13 Torr

With sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); palladium 10% on activated carbon; lithium methanolate; hydrogen; tri-n-butyl-tin hydride; phosphorus tribromide; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; toluene; 4.1: |Wittig Olefination;
DOI:10.1016/j.ejmech.2013.06.016