2,4,6-TRIMETHYLANISOLE

Base Information

• Chemical Name: 2,4,6-TRIMETHYLANISOLE
• CAS No.: 4028-66-4
• Molecular Formula: C10H14 O
• Molecular Weight: 150.221
• Hs Code.: 2909309090
• Mol file: 4028-66-4.mol

Synonyms:Anisole,2,4,6-trimethyl- (6CI,7CI,8CI); 2,4,6-Trimethylanisole;2-Methoxy-1,3,5-trimethylbenzene; Mesitylene methyl ether; Methoxymesitylene;Methyl 2,4,6-trimethylphenyl ether; Methyl mesityl ether

Chemical Property of 2,4,6-TRIMETHYLANISOLE

Chemical Property:

• Vapor Pressure: 0.352mmHg at 25°C
• Boiling Point: 205.8°Cat760mmHg
• Flash Point: 74°C
• PSA: 9.23000
• Density: 0.925g/cm³
• LogP: 2.62040

Purity/Quality:

97% ^*data from raw suppliers

2,4,6-Trimethylanisole ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,6-TRIMETHYLANISOLE

There total 13 articles about 2,4,6-TRIMETHYLANISOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,4,6-trimethylphenyl bromide (576-83-0) + sodium methylate (124-41-4) → 2,4,6-trimethylanisole (4028-66-4)

Guidance literature:

With methanol; Methyl formate; copper(l) chloride; at 115 ℃; for 2h; Autoclave; Green chemistry;

DOI:10.1007/s11164-014-1917-x

Reference yield: 90.0%

Mesitol (527-60-6) + methyl iodide (74-88-4) → 2,4,6-trimethylanisole (4028-66-4)

Guidance literature:

With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 13h;

DOI:10.1021/jm9900063

Reference yield: 89.0%

Mesitol (527-60-6) + dimethyl sulfate (77-78-1) → 2,4,6-trimethylanisole (4028-66-4)

Guidance literature:

With potassium hydroxide; In water; at 60 ℃; for 2h;

DOI:10.1002/1522-2675(20000906)83:9<2246::AID-HLCA2246>3.0.CO;2-X

upstream raw materials:

Mesitol

dimethyl sulfate

dimethylsulfonioacetate

6-acetoxy-2,4,6-trimethyl-cyclohexa-2,4-dienone

Downstream raw materials:

3-hydroxy-2,4,6-trimethylbenzaldehyde

bis(2-hydroxy-3,5-dimethylphenyl)ethane

1-Bromo-3-methoxy-2,4,6-trimethylbenzene

3,5-Bis-(chlormethyl)-2,4,6-trimethylanisol

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