3-tert-Butylsydnone

Base Information

Chemical Name:3-tert-Butylsydnone
CAS No.:6939-25-9
Molecular Formula:C₆H₁₀N₂O₂
Molecular Weight:142.158
Hs Code.:
NSC Number:56795
DSSTox Substance ID:DTXSID90219503
Wikidata:Q83096445

Synonyms:3-tert-butylsydnone

Suppliers and Price of 3-tert-Butylsydnone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-tert-Butylsydnone

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
XLogP3:2.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:142.074227566
Heavy Atom Count:10
Complexity:121

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(C)(C)[N+]1=NOC(=C1)[O-]

Technology Process of 3-tert-Butylsydnone

There total 3 articles about 3-tert-Butylsydnone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6939-24-8
N-nitroso-N-(t-butyl)glycine

: 6939-25-9
3-(t-butyl)sydnone

Guidance literature:: With acetic anhydride; at 100 ℃;

Reference yield:

: 37885-76-0
ethyl 2-(tert-butylamino)acetate

: 6939-25-9
3-(t-butyl)sydnone

Guidance literature:: Multi-step reaction with 3 steps

1: 10percent aq. NaOH / 0.75 h / Heating

2: conc. aq. HCl, aq. NaNO₂ / Ambient temperature

3: trifluoroacetic anhydride / ethyl acetate / 1 h / 0 °C

With hydrogenchloride; sodium hydroxide; trifluoroacetic anhydride; sodium nitrite; In ethyl acetate;
DOI:10.1002/jhet.5570330333

Reference yield:

: 58482-93-2
tert-butylaminoacetic acid

: 6939-25-9
3-(t-butyl)sydnone

Guidance literature:: Multi-step reaction with 2 steps

1: conc. aq. HCl, aq. NaNO₂ / Ambient temperature

2: trifluoroacetic anhydride / ethyl acetate / 1 h / 0 °C

With hydrogenchloride; trifluoroacetic anhydride; sodium nitrite; In ethyl acetate;
DOI:10.1002/jhet.5570330333