Mercury, chloro[5-iodo-2-[(phenylmethylene)amino]phenyl]-

Base Information

Chemical Name:Mercury, chloro[5-iodo-2-[(phenylmethylene)amino]phenyl]-
CAS No.:144271-83-0
Molecular Formula:C13H9ClHgIN
Molecular Weight:542.169
Hs Code.:

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Chemical Property of Mercury, chloro[5-iodo-2-[(phenylmethylene)amino]phenyl]-

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Technology Process of Mercury, chloro[5-iodo-2-[(phenylmethylene)amino]phenyl]-

There total 1 articles about Mercury, chloro[5-iodo-2-[(phenylmethylene)amino]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 3381-47-3,102904-39-2
N-benzylidene-4-iodoaniline

: 1600-27-7
mercury(II) diacetate

: 144271-83-0
2-(chloromercurio)-4-iodo-N-(benzylidene)aniline

Guidance literature:: With lithium chloride; In methanol; mixt. of Schiff base and Hg(OAc)2 (equal amts., concn. ca 0.1 M) in MeOH stirred and refluxed for 4 h, cooled to room temp.; addn. of LiCl soln.in hot MeOH; resulting thick mixt. stirred for about 10 min; ppt. filtered off, washed with ether, dried (vac.), crystn. from CHCl3; elem. anal.;
DOI:10.1021/om00059a058

Reference yield: 92.0%

: 7440-31-5
tin

: 144271-83-0
2-(chloromercurio)-4-iodo-N-(benzylidene)aniline

: dichlorobis{2-(benzylideneamino)-5-iodophenyl}tin(IV)

Guidance literature:: In xylene; the mercury compd. is heated with metallic tin to reflux in xylene for 2-10 h; after filtrn. the soln. is concd. by vac. distn. and cooled to room temp., filtered, washed with methanol and recrystd. from xylene, elem. anal.;
DOI:10.1016/0022-328X(93)83401-G