2,4,5-trichlorophenyl methylcarbamate

Base Information

Chemical Name:2,4,5-trichlorophenyl methylcarbamate
CAS No.:3942-57-2
Molecular Formula:C8H6 Cl3 N O2
Molecular Weight:254.4977
Hs Code.:

Synonyms:Carbamicacid, methyl-, 2,4,5-trichlorophenyl ester (6CI,7CI,8CI); Phenol,2,4,5-trichloro-, methylcarbamate (9CI); NSC 18115

Suppliers and Price of 2,4,5-trichlorophenyl methylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2,4,5-trichlorophenyl methylcarbamate

Chemical Property:

Vapor Pressure:0.000284mmHg at 25°C
Boiling Point:322.2°Cat760mmHg
Flash Point:148.7°C
Density:1.481g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,4,5-trichlorophenyl methylcarbamate

There total 4 articles about 2,4,5-trichlorophenyl methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 624-83-9
methyl isocyanate

: 95-95-4
2,4,5-trichlorophenol

: 3942-57-2
2,4,5-trichlorophenyl N-methylcarbamate

Guidance literature:: With pyridine; for 24h; Ambient temperature;
DOI:10.1021/jm00344a017

Reference yield: 79.0%

: 16947-69-6
2,4,5-Trichlorophenyl chloroformate

: 593-51-1
methylamine hydrochloride

: 3942-57-2
2,4,5-trichlorophenyl N-methylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 3 ℃; for 48h;
DOI:10.1055/s-1993-25809

Reference yield:

: 95-95-4
2,4,5-trichlorophenol

: 3942-57-2
2,4,5-trichlorophenyl N-methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / i-Pr₂EtN / CH₂Cl₂ / 1.) 0 deg C, 3 h, 2.) 0-20 deg C, 6 h, 3.) reflux, 2 h

2: 79 percent / i-Pr₂EtN / CH₂Cl₂ / 48 h / 0 - 3 °C

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1055/s-1993-25809