5-Benzoyl-3,5-dihydro-2lambda~6~-thieno[3,4-c]pyrrole-2,2(1H)-dione

Base Information

Chemical Name:5-Benzoyl-3,5-dihydro-2lambda~6~-thieno[3,4-c]pyrrole-2,2(1H)-dione
CAS No.:144425-38-7
Molecular Formula:C13H11NO3S
Molecular Weight:261.301
Hs Code.:
DSSTox Substance ID:DTXSID90576880
Wikidata:Q82466755

Synonyms:144425-38-7;5-Benzoyl-3,5-dihydro-2lambda~6~-thieno[3,4-c]pyrrole-2,2(1H)-dione;DTXSID90576880

Suppliers and Price of 5-Benzoyl-3,5-dihydro-2lambda~6~-thieno[3,4-c]pyrrole-2,2(1H)-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 5-Benzoyl-3,5-dihydro-2lambda~6~-thieno[3,4-c]pyrrole-2,2(1H)-dione

Chemical Property:

XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:261.04596439
Heavy Atom Count:18
Complexity:414

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CN(C=C2CS1(=O)=O)C(=O)C3=CC=CC=C3

Technology Process of 5-Benzoyl-3,5-dihydro-2lambda~6~-thieno[3,4-c]pyrrole-2,2(1H)-dione

There total 6 articles about 5-Benzoyl-3,5-dihydro-2lambda~6~-thieno[3,4-c]pyrrole-2,2(1H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 144425-34-3
5-benzoyl-3,4,5,6-tetrahydro-1H-thieno<3,4-c>pyrrole 2,2-dioxide

: 144425-38-7
5-benzoyl-3,5-dihydro-1H-thieno<3,4-c>pyrrole 2,2-dioxide

Guidance literature:: With manganese(IV) oxide; In benzene; for 96h; Ambient temperature;
DOI:10.1039/c39920001100

Reference yield:

: 50586-22-6
3,4,5,6-tetrahydro-1H-thieno[3,4-c]pyrrole 2,2-dioxide

: 144425-38-7
5-benzoyl-3,5-dihydro-1H-thieno<3,4-c>pyrrole 2,2-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / 40percent K₂CO₃ / CHCl₃ / 3 h

2: 54 percent / 'chemical manganese dioxide'-U / benzene / 96 h / Ambient temperature

With manganese(IV) oxide; potassium carbonate; In chloroform; benzene;
DOI:10.1016/0040-4020(94)00968-Z

Reference yield:

: 35105-74-9
5-benzyl-3,4,5,6-tetrahydro-1H-thieno[3,4-c]pyrrole 2,2-dioxide

: 144425-38-7
5-benzoyl-3,5-dihydro-1H-thieno<3,4-c>pyrrole 2,2-dioxide

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / 1,2-dichloro-ethane / 0 degC, 30 min, r.t., 3 h

2: 71 percent / MeOH / 1 h / 50 °C

3: 99 percent / 40percent K₂CO₃ / CHCl₃ / 3 h

4: 54 percent / 'chemical manganese dioxide'-U / benzene / 96 h / Ambient temperature

With methanol; manganese(IV) oxide; potassium carbonate; In chloroform; 1,2-dichloro-ethane; benzene;
DOI:10.1016/0040-4020(94)00968-Z