(2-methylcyclopent-1-en-1-yl)methyl 4-methylcyclohex-3-ene-1-carboxylate

Base Information

Chemical Name:(2-methylcyclopent-1-en-1-yl)methyl 4-methylcyclohex-3-ene-1-carboxylate
CAS No.:104762-26-7
Molecular Formula:C15H22 O2
Molecular Weight:234.334
Hs Code.:

Synonyms:3-Cyclohexene-1-carboxylicacid, 4-methyl-, (2-methyl-1-cyclopenten-1-yl)methyl ester, (?à)-

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2-methylcyclopent-1-en-1-yl)methyl 4-methylcyclohex-3-ene-1-carboxylate

Chemical Property:

Vapor Pressure:0.000326mmHg at 25°C
Boiling Point:320°Cat760mmHg
Flash Point:140.3°C
Density:1.021g/cm³

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2-methylcyclopent-1-en-1-yl)methyl 4-methylcyclohex-3-ene-1-carboxylate

There total 3 articles about (2-methylcyclopent-1-en-1-yl)methyl 4-methylcyclohex-3-ene-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 4342-60-3
4-methylcyclohex-3-enecarboxylic acid

: 81328-62-3
(2-methylcyclopent-1-enyl)methanol

: 104762-26-7
(2-methyl-1-cyclopentenyl)methyl 4-methyl-3-cyclohexene-1-carboxylate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1021/jo00375a054

Reference yield: 81.0%

: 81328-62-3
(2-methylcyclopent-1-enyl)methanol

: 16695-95-7
(4'-methylcyclohex-3'-ene-1-'-yl)carbonyl chloride

: 104762-26-7
(2-methyl-1-cyclopentenyl)methyl 4-methyl-3-cyclohexene-1-carboxylate

Guidance literature:: With pyridine; for 12h; Ambient temperature;
DOI:10.1021/jo00373a032

Reference yield:

: 67209-77-2
2-methyl-cyclopent-1-enecarboxylic acid

: 104762-26-7
(2-methyl-1-cyclopentenyl)methyl 4-methyl-3-cyclohexene-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

2: 82 percent / 4-(dimethylamino)pyridine, N,N-dicyclohexylcarbodiimide / CH₂Cl₂ / Ambient temperature

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane;
DOI:10.1021/jo00375a054