3-Bromo-3-phenylprop-2-enal

Base Information

Chemical Name:3-Bromo-3-phenylprop-2-enal
CAS No.:14804-59-2
Molecular Formula:C9H7BrO
Molecular Weight:211.058
Hs Code.:
DSSTox Substance ID:DTXSID60707907
Mol file:14804-59-2.mol

Synonyms:3-Bromo-3-phenylprop-2-enal;14804-59-2;2-Propenal, 3-bromo-3-phenyl-;DTXSID60707907

Suppliers and Price of 3-Bromo-3-phenylprop-2-enal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-Bromo-3-phenylprop-2-enal

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:209.96803
Heavy Atom Count:11
Complexity:157

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=CC=O)Br

Technology Process of 3-Bromo-3-phenylprop-2-enal

There total 8 articles about 3-Bromo-3-phenylprop-2-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 98-86-2
acetophenone

: 14804-59-2
3-bromo-3-phenylacrylaldehyde

Guidance literature:: N,N-dimethyl-formamide; With phosphorus tribromide; In chloroform; at 0 - 20 ℃; for 1.25h; Inert atmosphere;

acetophenone; In chloroform; at 20 ℃; Inert atmosphere;

With water; potassium carbonate; In chloroform; pH=8; Inert atmosphere; Cooling with ice;
DOI:10.1021/jo400950j

Reference yield: 75.0%

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 98-86-2
acetophenone

: 14804-59-2,33603-88-2
(Z)-β-bromocinnamaldehyde

Guidance literature:: N,N-dimethyl-formamide; With phosphorus tribromide; In chloroform; at 0 ℃; for 1h;

acetophenone; In chloroform; at 20 ℃; for 8h;
DOI:10.1021/ja062515h