Benzenebutanol, a-(phenylmethyl)-

Base Information

Chemical Name:Benzenebutanol, a-(phenylmethyl)-
CAS No.:149423-52-9
Molecular Formula:C17H20O
Molecular Weight:240.345
Hs Code.:

Synonyms:

Suppliers and Price of Benzenebutanol, a-(phenylmethyl)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenebutanol, a-(phenylmethyl)-

Chemical Property:

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Technology Process of Benzenebutanol, a-(phenylmethyl)-

There total 6 articles about Benzenebutanol, a-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5281-18-5
benzaldehyde, hydrazone

: 42238-15-3
4-phenyl-2-buten-1-ol

: 149423-52-9
1,5-diphenylpentan-2-ol

Guidance literature:: With potassium phosphate; tris(triphenylphosphine)ruthenium(II) chloride; 1,1'-bis(dicyclohexylphosphinocyclopentadienyl)iron; In 2-methyltetrahydrofuran; at 40 ℃; for 24h; Sealed tube; Inert atmosphere;
DOI:10.1002/anie.201915218

Reference yield:

: 54966-42-6
ethyl 4-phenylbut-2-enoate

: 149423-52-9
1,5-diphenylpentan-2-ol

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 °C / Inert atmosphere

2: tris(triphenylphosphine)ruthenium(II) chloride; 1,1'-bis(dicyclohexylphosphinocyclopentadienyl)iron; potassium phosphate / 2-methyltetrahydrofuran / 24 h / 40 °C / Sealed tube; Inert atmosphere

With potassium phosphate; tris(triphenylphosphine)ruthenium(II) chloride; 1,1'-bis(dicyclohexylphosphinocyclopentadienyl)iron; diisobutylaluminium hydride; In 2-methyltetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/anie.201915218