Benzenesulfenyl chloride, 4-(aminocarbonyl)-

Base Information

• Chemical Name: Benzenesulfenyl chloride, 4-(aminocarbonyl)-
• CAS No.: 150035-80-6
• Molecular Formula: C₇H₆ClNOS
• Molecular Weight: 187.65
• Mol file: 150035-80-6.mol

Synonyms:

Chemical Property of Benzenesulfenyl chloride, 4-(aminocarbonyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenesulfenyl chloride, 4-(aminocarbonyl)-

There total 1 articles about Benzenesulfenyl chloride, 4-(aminocarbonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-disulfanediyl-di-benzoic acid diamide (1227-29-8) → 4-carboxamidobenzensulfenyl chloride (150035-80-6)

Guidance literature:

With chlorine; In dichloromethane;

DOI:10.1002/jps.2600820515

Reference yield: 43.0%

4-carboxamidobenzensulfenyl chloride (150035-80-6) + 3-mercaptopropionic acid (107-96-0) → 3-(4-carboxamidophenyldithio)propionic acid

Guidance literature:

With acetic acid; for 2h; Heating;

DOI:10.1002/jps.2600820706

Reference yield: 40.0%

3-mercaptopropionitrile (1001-58-7) + 4-carboxamidobenzensulfenyl chloride (150035-80-6) → 4-(2-cyanoethyldithio)benzamide (149997-72-8)

Guidance literature:

In acetic acid; at 80 - 90 ℃; for 2h;

DOI:10.1002/jps.2600820515

upstream raw materials:

4,4'-disulfanediyl-di-benzoic acid diamide

Downstream raw materials:

4-(2-cyanoethyldithio)benzamide

ethyl 3-(4-carboxamidophenyldithio)propionthioimidate ester hydrochloride

Refernces