Phosphonic acid, [(phenyltelluro)methyl]-, diethyl ester

Base Information

Chemical Name:Phosphonic acid, [(phenyltelluro)methyl]-, diethyl ester
CAS No.:155934-75-1
Molecular Formula:C11H17O3PTe
Molecular Weight:355.828
Hs Code.:
DSSTox Substance ID:DTXSID30437340
Nikkaji Number:J2.215.763I
Wikidata:Q82252826

Synonyms:155934-75-1;Phosphonic acid, [(phenyltelluro)methyl]-, diethyl ester;DTXSID30437340;(Phenyltelluromethyl)phosphonic acid diethyl ester

Suppliers and Price of Phosphonic acid, [(phenyltelluro)methyl]-, diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Phosphonic acid, [(phenyltelluro)methyl]-, diethyl ester

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:357.9977541
Heavy Atom Count:16
Complexity:219

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=O)(C[Te]C1=CC=CC=C1)OCC

Technology Process of Phosphonic acid, [(phenyltelluro)methyl]-, diethyl ester

There total 4 articles about Phosphonic acid, [(phenyltelluro)methyl]-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 683-08-9
Diethyl methylphosphonate

: 55843-71-5
phenyltellurenyl bromide

: 155934-75-1
diethyl (phenyltelluromethyl)phosphonate

Guidance literature:: With lithium diisopropyl amide;
DOI:10.1016/0040-4039(95)01656-2

Reference yield:

: 32294-60-3
diphenyl ditelluride

: 155934-75-1
diethyl (phenyltelluromethyl)phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Br₂

2.1: LDA / tetrahydrofuran

2.2: tetrahydrofuran

With bromine; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/j.tet.2005.05.085

Reference yield:

: 683-08-9
Diethyl methylphosphonate

: 55843-74-8
phenyltellurenyl iodide

: 155934-75-1
diethyl (phenyltelluromethyl)phosphonate

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h, 2.) -78 deg C, 1 h; -78 deg C -> room temperature, 1 h;