1,1'-(1-Iodoethene-1,2-diyl)dibenzene

Base Information

Chemical Name:1,1'-(1-Iodoethene-1,2-diyl)dibenzene
CAS No.:156181-20-3
Molecular Formula:C14H11I
Molecular Weight:306.146
Hs Code.:
DSSTox Substance ID:DTXSID30705733

Synonyms:1,1'-(1-Iodoethene-1,2-diyl)dibenzene;156181-20-3;SCHEMBL5574065;DTXSID30705733

Suppliers and Price of 1,1'-(1-Iodoethene-1,2-diyl)dibenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1,1'-(1-Iodoethene-1,2-diyl)dibenzene

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:305.99055
Heavy Atom Count:15
Complexity:207

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=C(C2=CC=CC=C2)I

Technology Process of 1,1'-(1-Iodoethene-1,2-diyl)dibenzene

There total 4 articles about 1,1'-(1-Iodoethene-1,2-diyl)dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-65-5
diphenyl acetylene

: 451-40-1
phenyl benzyl ketone

: 119379-68-9
(E)-1,1'-(1-Iodo-1,2-ethenediyl)bisbenzene

: 156181-20-3
(Z)-1,1'-(1-Iodo-1,2-ethenediyl)bisbenzene

Guidance literature:: With silica gel; phosphorous triiodide; In dichloromethane; for 3h; Product distribution; various reaction times and adsorbent;
DOI:10.1021/jo00090a031

Reference yield:

: 119379-68-9
(E)-1,1'-(1-Iodo-1,2-ethenediyl)bisbenzene

: 156181-20-3
(Z)-1,1'-(1-Iodo-1,2-ethenediyl)bisbenzene

Guidance literature:: With silica gel; phosphorous triiodide; In dichloromethane; for 24h; Yield given;
DOI:10.1021/jo00090a031

Reference yield:

: 501-65-5
diphenyl acetylene

: 156181-20-3
(Z)-1,1'-(1-Iodo-1,2-ethenediyl)bisbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / AcI, silica gel / CH₂Cl₂ / 1 h

2: PI₃, silica gel / CH₂Cl₂ / 24 h

With acetyl iodide; silica gel; phosphorous triiodide; In dichloromethane;
DOI:10.1021/jo00090a031