Ethanone, 2-bromo-1-[3-(2-phenylethyl)-2-benzofuranyl]-

Base Information

Chemical Name:Ethanone, 2-bromo-1-[3-(2-phenylethyl)-2-benzofuranyl]-
CAS No.:158358-17-9
Molecular Formula:C18H15BrO2
Molecular Weight:343.22
Hs Code.:
DSSTox Substance ID:DTXSID80447459
Wikidata:Q82266337
Mol file:158358-17-9.mol

Synonyms:158358-17-9;2-bromo-1-(3-phenethylbenzofuran-2-yl)ethanone;Ethanone, 2-bromo-1-[3-(2-phenylethyl)-2-benzofuranyl]-;DTXSID80447459

Suppliers and Price of Ethanone, 2-bromo-1-[3-(2-phenylethyl)-2-benzofuranyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Ethanone, 2-bromo-1-[3-(2-phenylethyl)-2-benzofuranyl]-

Chemical Property:

XLogP3:5.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:342.02554
Heavy Atom Count:21
Complexity:351

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CCC2=C(OC3=CC=CC=C32)C(=O)CBr

Technology Process of Ethanone, 2-bromo-1-[3-(2-phenylethyl)-2-benzofuranyl]-

There total 1 articles about Ethanone, 2-bromo-1-[3-(2-phenylethyl)-2-benzofuranyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 158358-16-8
1-(3-phenylethylbenzofuran-2-yl)ethan-1-one

: 158358-17-9
2-bromo-1-(3-phenethyl-benzofuran-2-yl)ethanone

Guidance literature:: With acetic acid; pyridinium hydrobromide perbromide; at 50 - 55 ℃; for 4h;
DOI:10.1016/S0957-4166(03)00276-3

Reference yield: 90.0%

: 158358-17-9
2-bromo-1-(3-phenethyl-benzofuran-2-yl)ethanone

: (S)-(+)-2-bromo-1-(3-phenethyl-benzofuran-2-yl)ethanol

Guidance literature:: With formic acid; RhCl[(R,R)-TsDPEN](C₅Me₅); triethylamine; In ethyl acetate; at 20 ℃; for 168h;
DOI:10.1016/j.tetasy.2005.08.012

Reference yield:

: 158358-17-9
2-bromo-1-(3-phenethyl-benzofuran-2-yl)ethanone

: 2-[4-(4-Methoxy-phenyl)-piperazin-1-yl]-1-(3-phenethyl-benzofuran-2-yl)-ethanol

Guidance literature:: Multi-step reaction with 5 steps

1: LiAlH₄

2: p-TSA

4: etheral HCl

5: 93 percent / NaBH₄ / methanol

With hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; toluene-4-sulfonic acid; In methanol;
DOI:10.1021/jm960384x