1H-Benzimidazole, 1-benzoyl-5,6-dimethyl-

Base Information

Chemical Name:1H-Benzimidazole, 1-benzoyl-5,6-dimethyl-
CAS No.:16109-46-9
Molecular Formula:C16H14N2O
Molecular Weight:250.3
Hs Code.:
DSSTox Substance ID:DTXSID50363778
Nikkaji Number:J3.376.614I
Wikidata:Q82147515
Mol file:16109-46-9.mol

Synonyms:16109-46-9;1H-Benzimidazole, 1-benzoyl-5,6-dimethyl-;Oprea1_466945;(5,6-dimethyl-1H-benzimidazol-1-yl)(phenyl)methanone;DTXSID50363778;STK095276;AKOS001721201;1-benzoyl-5,6-dimethyl-1H-benzimidazole;SR-01000511011;Phenyl(5,6-dimethyl-1H-benzoimidazole-1-yl) ketone;SR-01000511011-1;(5,6-dimethyl-1H-1,3-benzimidazol-1-yl)(phenyl)methanone

Suppliers and Price of 1H-Benzimidazole, 1-benzoyl-5,6-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 1H-Benzimidazole, 1-benzoyl-5,6-dimethyl-

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:250.110613074
Heavy Atom Count:19
Complexity:338

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1C)N(C=N2)C(=O)C3=CC=CC=C3

Technology Process of 1H-Benzimidazole, 1-benzoyl-5,6-dimethyl-

There total 4 articles about 1H-Benzimidazole, 1-benzoyl-5,6-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 582-60-5
5,6-dimethyl-1H-benzo[d]imida-zole

: 100-52-7
benzaldehyde

: 16109-46-9
(5,6-dimethyl-1H-benzo[d]imidazol-1-yl)(phenyl)methanone

Guidance literature:: With di-tert-butyl peroxide; In ethyl acetate; at 110 ℃; for 15h; Reagent/catalyst; Solvent; Temperature; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2014.07.009

Reference yield: 82.0%

: 582-60-5
5,6-dimethyl-1H-benzo[d]imida-zole

: 98-88-4
benzoyl chloride

: 16109-46-9
(5,6-dimethyl-1H-benzo[d]imidazol-1-yl)(phenyl)methanone

Guidance literature:: With triethylamine; In chloroform; for 1h; Ambient temperature;
DOI:10.1021/jo00186a016

Reference yield: 63.0%

: 103-82-2
phenylacetic acid

: 582-60-5
5,6-dimethyl-1H-benzo[d]imida-zole

: 16109-46-9
(5,6-dimethyl-1H-benzo[d]imidazol-1-yl)(phenyl)methanone

Guidance literature:: With pyridine; oxygen; copper(I) bromide; In o-xylene; at 130 ℃; for 24h; under 760.051 Torr; chemoselective reaction; Sealed tube;
DOI:10.1039/c6ob01167e